Technology Process of Cycloheptanone, 3-methyl-6-(1-methylethenyl)-
There total 3 articles about Cycloheptanone, 3-methyl-6-(1-methylethenyl)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
2,6-dimethylpyridine; silver trifluoromethanesulfonate;
In
dichloromethane;
at 20 ℃;
for 0.5h;
Overall yield = 67 %; Overall yield = 39.6 mg;
Inert atmosphere;
DOI:10.1002/chem.201900497
- Guidance literature:
-
Multi-step reaction with 3 steps
1.1: diisopropylamine; n-butyllithium / tetrahydrofuran; hexane / 1.08 h / -78 °C / Inert atmosphere
1.2: 1 h / -78 °C / Inert atmosphere
2.1: N-iodo-succinimide / dichloromethane / 0.75 h / -78 °C / Inert atmosphere
3.1: silver trifluoromethanesulfonate; 2,6-dimethylpyridine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
With
2,6-dimethylpyridine; N-iodo-succinimide; n-butyllithium; silver trifluoromethanesulfonate; diisopropylamine;
In
tetrahydrofuran; hexane; dichloromethane;
DOI:10.1002/chem.201900497
- Guidance literature:
-
Multi-step reaction with 2 steps
1: N-iodo-succinimide / dichloromethane / 0.75 h / -78 °C / Inert atmosphere
2: silver trifluoromethanesulfonate; 2,6-dimethylpyridine / dichloromethane / 0.5 h / 20 °C / Inert atmosphere
With
2,6-dimethylpyridine; N-iodo-succinimide; silver trifluoromethanesulfonate;
In
dichloromethane;
DOI:10.1002/chem.201900497
