4-chloro-N-(4-methylphenyl)-2-nitroaniline

Base Information

• Chemical Name: 4-chloro-N-(4-methylphenyl)-2-nitroaniline
• CAS No.: 32724-91-7
• Molecular Formula: C13H11 Cl N2 O2
• Molecular Weight: 262.696
• Mol file: 32724-91-7.mol

Synonyms:p-Toluidine,N-(4-chloro-2-nitrophenyl)- (6CI,7CI,8CI);4-Chloro-4'-methyl-2-nitrodiphenylamine; NSC 369143

Chemical Property of 4-chloro-N-(4-methylphenyl)-2-nitroaniline

Chemical Property:

• Vapor Pressure: 4.15E-06mmHg at 25°C
• Boiling Point: 384.3°Cat760mmHg
• Flash Point: 186.2°C
• Density: 1.343g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 4-chloro-N-(4-methylphenyl)-2-nitroaniline

There total 3 articles about 4-chloro-N-(4-methylphenyl)-2-nitroaniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-toluidine (106-49-0,12221-03-3) + 2,5-dichloronitrobenzene (89-61-2) → (4-chloro-2-nitro-phenyl)-p-tolyl-amine (32724-91-7)

Guidance literature:

With sodium acetate;

DOI:10.1021/jo01375a013

Reference yield:

p-toluidine (106-49-0,12221-03-3) → (4-chloro-2-nitro-phenyl)-p-tolyl-amine (32724-91-7)

Guidance literature:

With triethylamine; In tetrahydrofuran;

DOI:10.1016/j.bmcl.2010.10.131

Reference yield:

→ (4-chloro-2-nitro-phenyl)-p-tolyl-amine (32724-91-7)

Guidance literature:

2,5-Dichlornitrobenzol, p-Toluidin;

upstream raw materials:

p-toluidine

2,5-dichloronitrobenzene

Downstream raw materials:

C₂₂H₁₇ClN₂O₂

C₁₆H₁₃ClN₂O₂

C₁₃H₁₃ClN₂

C₂₆H₂₄ClN₃O₃