3-Pyridinecarboxylic acid, 5-[bis(2-butenyloxy)phosphinyl]-1,4-dihydro-2,6-dimethyl-4-(3-nitrophen yl)-, 2-[methyl(phenylmethyl)amino]ethyl ester

Base Information

Chemical Name:3-Pyridinecarboxylic acid, 5-[bis(2-butenyloxy)phosphinyl]-1,4-dihydro-2,6-dimethyl-4-(3-nitrophen yl)-, 2-[methyl(phenylmethyl)amino]ethyl ester
CAS No.:112057-18-8
Molecular Formula:C₃₂H₄₀N₃O₇P
Molecular Weight:609.659
Hs Code.:

3-Pyridinecarboxylic acid,
5-[bis(2-butenyloxy)phosphinyl]-1,4-dihydro-2,6-dimethyl-4-(3-nitrophen
yl)-, 2-[methyl(phenylmethyl)amino]ethyl ester

Synonyms:

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Chemical Property of 3-Pyridinecarboxylic acid, 5-[bis(2-butenyloxy)phosphinyl]-1,4-dihydro-2,6-dimethyl-4-(3-nitrophen yl)-, 2-[methyl(phenylmethyl)amino]ethyl ester

Chemical Property:

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Technology Process of 3-Pyridinecarboxylic acid, 5-[bis(2-butenyloxy)phosphinyl]-1,4-dihydro-2,6-dimethyl-4-(3-nitrophen yl)-, 2-[methyl(phenylmethyl)amino]ethyl ester

There total 4 articles about 3-Pyridinecarboxylic acid, 5-[bis(2-butenyloxy)phosphinyl]-1,4-dihydro-2,6-dimethyl-4-(3-nitrophen yl)-, 2-[methyl(phenylmethyl)amino]ethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 2.0%

: 54527-73-0
2-ethyl 3-aminocrotonate

: 112057-39-3
{1-[1-(3-Nitro-phenyl)-meth-(Z)-ylidene]-2-oxo-propyl}-phosphonic acid bis-((Z)-but-2-enyl) ester

: 112057-18-8
5-{Bis-[((Z)-but-2-enyl)oxy]-phosphoryl}-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid 2-(benzyl-methyl-amino)-ethyl ester

Guidance literature:: In isopropyl alcohol; Heating;
DOI:10.1248/cpb.35.3898

Reference yield:

: 99-61-6
3-nitro-benzaldehyde

: 112057-18-8
5-{Bis-[((Z)-but-2-enyl)oxy]-phosphoryl}-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid 2-(benzyl-methyl-amino)-ethyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: piperidine-AcOH salt / benzene / Heating

2: 2 percent / propan-2-ol / Heating

With piperdinium acetate; In isopropyl alcohol; benzene;
DOI:10.1248/cpb.35.3898

Reference yield:

: 51666-84-3
Phosphorous acid tris-((E)-but-2-enyl) ester

: 112057-18-8
5-{Bis-[((Z)-but-2-enyl)oxy]-phosphoryl}-2,6-dimethyl-4-(3-nitro-phenyl)-1,4-dihydro-pyridine-3-carboxylic acid 2-(benzyl-methyl-amino)-ethyl ester

Guidance literature:: Multi-step reaction with 3 steps

1: 41 percent / 120 °C

2: piperidine-AcOH salt / benzene / Heating

3: 2 percent / propan-2-ol / Heating

With piperdinium acetate; In isopropyl alcohol; benzene;
DOI:10.1248/cpb.35.3898