Stannane, [2-(1-methoxycyclohexyl)-1-(trimethylplumbyl)ethenyl]trimethyl-, (Z)-

Base Information

• Chemical Name: Stannane, [2-(1-methoxycyclohexyl)-1-(trimethylplumbyl)ethenyl]trimethyl-, (Z)-
• CAS No.: 112166-72-0
• Molecular Formula: C₁₅H₃₂OPbSn
• Molecular Weight: 554.328

Synonyms:

Chemical Property of Stannane, [2-(1-methoxycyclohexyl)-1-(trimethylplumbyl)ethenyl]trimethyl-, (Z)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Stannane, [2-(1-methoxycyclohexyl)-1-(trimethylplumbyl)ethenyl]trimethyl-, (Z)-

There total 2 articles about Stannane, [2-(1-methoxycyclohexyl)-1-(trimethylplumbyl)ethenyl]trimethyl-, (Z)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

((CH2)5C(CH3O))HCC(Sn(CH3)3)2 (103670-89-9) + trimethyllead chloride (1520-78-1) → CH3O(C6H10)CHC(Sn(CH3)3)Pb(CH3)3 (112166-71-9,112166-72-0) + CH3O(C6H10)CHC(Sn(CH3)3)Pb(CH3)3 (112166-71-9,112166-72-0)

Guidance literature:

With methyllithium; In tetrahydrofuran; equimolar mixt. of distannylalkene and MeLi in THF was stirred at -78°C for 1-2 h under Ar, added to 1 equiv of Me3PbCl in THF, stirred for 1 h at -78°C, allowed to warm to room temp.; total yield 71%,E/Z ratio 80:20 ((1)H NMR data); water was added, org. phase sepd., dried, solvent removed, residue was distilled in vacuo;

DOI:10.1016/0022-328X(87)85003-9

Reference yield:

((CH2)5C(CH3O))HCC(Sn(CH3)3)2 (103670-89-9) + trimethyllead chloride (1520-78-1) → CH3O(C6H10)CHC(Sn(CH3)3)Pb(CH3)3 (112166-71-9,112166-72-0) + CH3O(C6H10)CHC(Sn(CH3)3)Pb(CH3)3 (112166-71-9,112166-72-0)

Guidance literature:

With methyllithium; In tetrahydrofuran; equimolar mixt. of distannylalkene and MeLi in THF was stirred at -78°C for 1-2 h under Ar, added to 1 equiv of Me3PbCl in THF, stirred for 1 h at -78°C, allowed to warm to room temp.; total yield 71%,E/Z ratio 80:20 ((1)H NMR data); water was added, org. phase sepd., dried, solvent removed, residue was distilled in vacuo;

DOI:10.1016/0022-328X(87)85003-9

upstream raw materials:

((CH₂)5C(CH₃O))HCC(Sn(CH₃)3)2

trimethyllead chloride

Post a RFQ

Cas No.:

Product Name:

Quantity:

Please select Metric Ton KG G Pound L ML

Email:

Company name:

Valid Period:

Detailed Requirements:

• Sample
• MOQ
• GMP
• FDA
• Price
  FOB CIF CFR EXW
• Urgent purchase

Enter 15 to 2000 letters.Word count: 0 letters

Attach files(File Format: Jpeg, Jpg, Gif, Png, PDF, PPT, Zip, Rar,Word or Excel Maximum File Size: 3MB)

Remove

Submit

1

What can I do for you?
Get Best Price

Get Best Price for 112166-72-0 Stannane, [2-(1-methoxycyclohexyl)-1-(trimethylplumbyl)ethenyl]trimethyl-, (Z)-

Send

Send

Metric Ton KG G Pound L ML

Send

Send