Trigermane, 1,1,1,2,3,3,3-heptaphenyl-2-(triphenylgermyl)-

Base Information

Chemical Name:Trigermane, 1,1,1,2,3,3,3-heptaphenyl-2-(triphenylgermyl)-
CAS No.:112168-56-6
Molecular Formula:C₆₀H₅₀Ge₄
Molecular Weight:1061.42
Hs Code.:

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Trigermane, 1,1,1,2,3,3,3-heptaphenyl-2-(triphenylgermyl)-

Chemical Property:

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of Trigermane, 1,1,1,2,3,3,3-heptaphenyl-2-(triphenylgermyl)-

There total 1 articles about Trigermane, 1,1,1,2,3,3,3-heptaphenyl-2-(triphenylgermyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 2875-92-5
phenylgermane

: N,N-dimethyltriphenylgermylamine

: 112168-56-6
PhGe(GePh₃)3

Guidance literature:: In acetonitrile; byproducts: Me2NH, CH3CN; (N2); std. Schlenk technique; soln. of Ph3GeNMe2 (3 equiv.) in MeCN was added to soln. of PhGeH3 in MeCN; sealed; heated in bath 85°C for48 h; cooled; solvent removed (vac.); distd. (135°C, 0.01 torr); elem. anal.;
DOI:10.1021/om800040f

Reference yield: 80.0%

: 112168-56-6
PhGe(GePh₃)3

: 1493-13-6
trifluorormethanesulfonic acid

: 139599-12-5
triphenylgermanetriflate

Guidance literature:: In chloroform-d1; byproducts: C6H6; (N2); std. Schlenk technique; acid (1 equiv.) was added to soln. of Ge compd. in CDCl3; kept at room temp. for 4 h; NMR monitoring; volatiles removed (vac.);
DOI:10.1021/om800040f

Reference yield:

: 112168-56-6
PhGe(GePh₃)3

: 2816-38-8
(Ph₃Ge)3GeH

Guidance literature:: Multi-step reaction with 2 steps

1: chloroform-d1

2: diethyl ether

In diethyl ether; chloroform-d1;
DOI:10.1021/om800040f