N-(7H-purin-6-yldiazenyl)aniline

Base Information

Chemical Name:N-(7H-purin-6-yldiazenyl)aniline
CAS No.:112177-85-2
Molecular Formula:C₁₁H₉N₇
Molecular Weight:239.239
Hs Code.:
DSSTox Substance ID:DTXSID10404070
NSC Number:352721

Synonyms:N-(7H-purin-6-yldiazenyl)aniline;112177-85-2;DTXSID10404070;NSC352721;NSC-352721

Suppliers and Price of N-(7H-purin-6-yldiazenyl)aniline

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(7H-purin-6-yldiazenyl)aniline

Chemical Property:

XLogP3:2.5
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:6
Rotatable Bond Count:3
Exact Mass:239.09194332
Heavy Atom Count:18
Complexity:289

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:C1=CC=C(C=C1)NN=NC2=NC=NC3=C2NC=N3

Technology Process of N-(7H-purin-6-yldiazenyl)aniline

There total 5 articles about N-(7H-purin-6-yldiazenyl)aniline which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 11.0%

: 60285-31-6
N,N'-diphenyl-N-nitroso-urea

: 66224-66-6,66224-67-7,66224-68-8,66224-69-9,134434-48-3,134434-49-4,134454-76-5,134461-75-9
adenine

: 112177-85-2
(E)-6-(3-Phenyl-2-triazen-1-yl)purine

Guidance literature:: With sodium hydroxide; at 0 ℃; for 0.666667h;
DOI:10.1248/cpb.32.564

Reference yield:

: 77070-97-4
(E)-6-<3-(4-Bromophenyl)-2-triazen-1-yl>purine

: 112177-85-2
(E)-6-(3-Phenyl-2-triazen-1-yl)purine

Guidance literature:: Multi-step reaction with 2 steps

1: 5 percent / sodium dithionite / aq. NaOH / 1.) room temp., 2 h, 2.) 50 deg C, 14 h, 3.) 100 deg C, 15 min

2: 1.) conc. HCl, NaNO₂, 2.) NaOH / 1.) H₂O, 0 deg C, 2.) pH 10-11, 15 min

With hydrogenchloride; sodium hydroxide; sodium dithionite; sodium nitrite; In sodium hydroxide;
DOI:10.1021/jo00324a001

Reference yield:

: 112177-84-1
N¹-(p-methylphenyl)-N³-purinyltriazene

: 112177-85-2
(E)-6-(3-Phenyl-2-triazen-1-yl)purine

Guidance literature:: Multi-step reaction with 2 steps

1: aq. NaOH / 72 h / 60 - 100 °C / pH 10

2: 1.) conc. HCl, NaNO₂, 2.) NaOH / 1.) H₂O, 0 deg C, 2.) pH 10-11, 15 min

With hydrogenchloride; sodium hydroxide; sodium nitrite;
DOI:10.1021/jo00324a001