4-((1E)-3-Hydroxy-1-propenyl)-2-(3-methyl-2-butenyl)phenol

Base Information

Chemical Name:4-((1E)-3-Hydroxy-1-propenyl)-2-(3-methyl-2-butenyl)phenol
CAS No.:104358-48-7
Molecular Formula:C₁₄H₁₈O₂
Molecular Weight:218.296
Hs Code.:
Nikkaji Number:J2.518.235I
Metabolomics Workbench ID:129568
ChEMBL ID:CHEMBL252311
Mol file:104358-48-7.mol

Synonyms:4-((1E)-3-Hydroxy-1-propenyl)-2-(3-methyl-2-butenyl)phenol;Phenol, 4-((1E)-3-hydroxy-1-propenyl)-2-(3-methyl-2-butenyl)-;104358-48-7;CHEMBL252311;4-hydroxy-3-(3-methyl-2-butenyl)cinnamyl alcohol

Suppliers and Price of 4-((1E)-3-Hydroxy-1-propenyl)-2-(3-methyl-2-butenyl)phenol

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
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Total 0 raw suppliers

Chemical Property of 4-((1E)-3-Hydroxy-1-propenyl)-2-(3-methyl-2-butenyl)phenol

Chemical Property:

Vapor Pressure:2.33E-06mmHg at 25°C
Boiling Point:377.2°C at 760 mmHg
Flash Point:178.6°C
Density:1.08g/cm³
XLogP3:3.3
Hydrogen Bond Donor Count:2
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:4
Exact Mass:218.130679813
Heavy Atom Count:16
Complexity:252

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(=CCC1=C(C=CC(=C1)C=CCO)O)C
Isomeric SMILES:CC(=CCC1=C(C=CC(=C1)/C=C/CO)O)C

Technology Process of 4-((1E)-3-Hydroxy-1-propenyl)-2-(3-methyl-2-butenyl)phenol

There total 3 articles about 4-((1E)-3-Hydroxy-1-propenyl)-2-(3-methyl-2-butenyl)phenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

: 72704-01-9
(E)-methyl 3-[4-Hydroxy-3-(3-methylbut-2-en-1-yl)phenyl]acrylate

: 104358-48-7
4-hydroxy-3-(3-methyl-2-butenyl)-cinnamyl alcohol

Guidance literature:: With diisobutylaluminium hydride; In toluene; at 0 ℃; for 4.5h;
DOI:10.1021/np980304n

Reference yield:

: 7400-08-0,50940-26-6
p-Coumaric Acid

: 104358-48-7
4-hydroxy-3-(3-methyl-2-butenyl)-cinnamyl alcohol

Guidance literature:: Multi-step reaction with 3 steps

1: 63 percent / H₂SO₄ / Heating

2: 1.) NaH / 1.) toluene, 60 - 65 deg C, 3.5 h, 2.) 35 deg C, 72 h.

3: 73 percent / DIBAL-H / toluene / 4.5 h / 0 °C

With sulfuric acid; sodium hydride; diisobutylaluminium hydride; In toluene;
DOI:10.1021/np980304n

Reference yield:

: 3943-97-3
methyl 4-hydroxycinnamate

: 104358-48-7
4-hydroxy-3-(3-methyl-2-butenyl)-cinnamyl alcohol

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) NaH / 1.) toluene, 60 - 65 deg C, 3.5 h, 2.) 35 deg C, 72 h.

2: 73 percent / DIBAL-H / toluene / 4.5 h / 0 °C

With sodium hydride; diisobutylaluminium hydride; In toluene;
DOI:10.1021/np980304n