2-Propenoic acid, 16-bromohexadecyl ester

Base Information

• Chemical Name: 2-Propenoic acid, 16-bromohexadecyl ester
• CAS No.: 112231-61-5
• Molecular Formula: C19H35BrO2
• Molecular Weight: 375.39
• Mol file: 112231-61-5.mol

Synonyms:

Chemical Property of 2-Propenoic acid, 16-bromohexadecyl ester

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of 2-Propenoic acid, 16-bromohexadecyl ester

There total 1 articles about 2-Propenoic acid, 16-bromohexadecyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

16-bromohexadecan-1-ol (59101-28-9) + acryloyl chloride (814-68-6,25189-84-8) → Acrylic acid 16-bromo-hexadecyl ester (112231-61-5)

Guidance literature:

With triethylamine; In dichloromethane; Ambient temperature;

DOI:10.1021/ja00250a036

Reference yield:

Acrylic acid 16-bromo-hexadecyl ester (112231-61-5) → hexadecyl acrylate (13402-02-3,25986-78-1)

Guidance literature:

Multi-step reaction with 2 steps

1: sodium iodide / butan-2-one / 3 h / Heating

2: 19 percent / tertbutyltin hydride, AIBN / benzene / 3 h / Heating

With 2,2'-azobis(isobutyronitrile); tertbutyltin hydride; sodium iodide; In butanone; benzene;

DOI:10.1021/ja00250a036

upstream raw materials:

16-bromohexadecan-1-ol

acryloyl chloride

Downstream raw materials:

hexadecyl acrylate