Phosphonium, tetrakis(4-methylphenyl)-, iodide

Base Information

Chemical Name:Phosphonium, tetrakis(4-methylphenyl)-, iodide
CAS No.:112368-29-3
Molecular Formula:C28H28P.I
Molecular Weight:522.409
Hs Code.:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phosphonium, tetrakis(4-methylphenyl)-, iodide

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Technology Process of Phosphonium, tetrakis(4-methylphenyl)-, iodide

There total 4 articles about Phosphonium, tetrakis(4-methylphenyl)-, iodide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 624-31-7
4-tolyl iodide

: 112368-29-3
tetrakis(4-methylphenyl)phosphonium iodide,

Guidance literature:: With white phosphorus; 1,3-dicyano-5-fluoro-2,4,6-tris(diphenylamino)benzene; triethylamine; In acetonitrile; benzene; for 24h; Inert atmosphere; Glovebox; Sealed tube; Irradiation;
DOI:10.1002/chem.202002646

Reference yield:

: 2417-95-0
p-tolyllithium

: 112368-29-3
tetrakis(4-methylphenyl)phosphonium iodide,

Guidance literature:: Multi-step reaction with 2 steps

1: PCl₃ / -20 °C

2: palladium acetate / xylene / 3 h / Heating

With phosphorus trichloride; palladium diacetate; In xylene;
DOI:10.1039/DT9880000277