Stannane, tricyclohexyl[(2-thienylcarbonyl)oxy]-

Base Information

Chemical Name:Stannane, tricyclohexyl[(2-thienylcarbonyl)oxy]-
CAS No.:112379-61-0
Molecular Formula:C₂₃H₃₆O₂SSn
Molecular Weight:495.314
Hs Code.:

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Chemical Property of Stannane, tricyclohexyl[(2-thienylcarbonyl)oxy]-

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Technology Process of Stannane, tricyclohexyl[(2-thienylcarbonyl)oxy]-

There total 1 articles about Stannane, tricyclohexyl[(2-thienylcarbonyl)oxy]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 3091-32-5
tricyclohexyltin(IV) chloride

: 25112-68-9
2-thiophenecarboxylic acid sodium salt

: 112379-61-0
(C₆H₁₁)3Sn(SCHCHCHCCOO)

Guidance literature:: In ethanol; byproducts: sodium chloride; to soln. of Sn-compd. in abs. alc. was added ligand, mixt. refluxed for 3-4 h, concd. to half the vol., mixt. cooled, NaCl filtered, benzene added, mixt. refluxed for 2 h (trap), NaCl filtered, repetition of procedure until NaCl is completely removed; solvents were removed completely, residue dried in vacuo; complex recrystd. from ethanol; elem. anal.;
DOI:10.1016/S0277-5387(00)81029-3