Benzoic acid, 2-[[2-hydroxy-6-methyl-3-(1-methylethyl)benzoyl]oxy]-6-methyl-3-(1-meth ylethyl)-, 2-carboxy-6-(1-methylethyl)phenyl ester

Base Information

• Chemical Name: Benzoic acid, 2-[[2-hydroxy-6-methyl-3-(1-methylethyl)benzoyl]oxy]-6-methyl-3-(1-meth ylethyl)-, 2-carboxy-6-(1-methylethyl)phenyl ester
• CAS No.: 112404-77-0
• Molecular Formula: C32H36O7
• Molecular Weight: 532.634
• Mol file: 112404-77-0.mol

Synonyms:

Chemical Property of Benzoic acid, 2-[[2-hydroxy-6-methyl-3-(1-methylethyl)benzoyl]oxy]-6-methyl-3-(1-meth ylethyl)-, 2-carboxy-6-(1-methylethyl)phenyl ester

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of Benzoic acid, 2-[[2-hydroxy-6-methyl-3-(1-methylethyl)benzoyl]oxy]-6-methyl-3-(1-meth ylethyl)-, 2-carboxy-6-(1-methylethyl)phenyl ester

There total 20 articles about Benzoic acid, 2-[[2-hydroxy-6-methyl-3-(1-methylethyl)benzoyl]oxy]-6-methyl-3-(1-meth ylethyl)-, 2-carboxy-6-(1-methylethyl)phenyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

C46H48O7 (112404-59-8) → C32H36O7 (112404-77-0)

Guidance literature:

With hydrogen; palladium on activated charcoal; In ethyl acetate; under 1520 Torr; Yield given; Ambient temperature;

DOI:10.1016/S0040-4020(01)90268-6

Reference yield:

3-isopropyl-6-methylsalicylic acid (548-51-6) → C32H36O7 (112404-77-0)

Guidance literature:

Multi-step reaction with 6 steps

1: 81.7 percent / KF / dimethylformamide / Ambient temperature

3: 37 percent / Zn/HCl / tetrahydrofuran / 1 h

4: 1-chloro-N,N,2-trimethylpropenylamine / CH₂Cl₂ / 1.5 h / Ambient temperature

5: 1.62 g / NaH / diethyl ether / Ambient temperature

6: H₂ / 10percent Pd/C / ethyl acetate / 1520 Torr / Ambient temperature

With hydrogenchloride; potassium fluoride; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; hydrogen; sodium hydride; zinc; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)90268-6

Reference yield:

thymol 2-tetrahydropyranyl ether (112404-79-2) → C32H36O7 (112404-77-0)

Guidance literature:

Multi-step reaction with 7 steps

2: 81.7 percent / KF / dimethylformamide / Ambient temperature

4: 37 percent / Zn/HCl / tetrahydrofuran / 1 h

5: 1-chloro-N,N,2-trimethylpropenylamine / CH₂Cl₂ / 1.5 h / Ambient temperature

6: 1.62 g / NaH / diethyl ether / Ambient temperature

7: H₂ / 10percent Pd/C / ethyl acetate / 1520 Torr / Ambient temperature

With hydrogenchloride; potassium fluoride; 1-chloro-1-(dimethylamino)-2-methyl-1-propene; hydrogen; sodium hydride; zinc; palladium on activated charcoal; In tetrahydrofuran; diethyl ether; dichloromethane; ethyl acetate; N,N-dimethyl-formamide;

DOI:10.1016/S0040-4020(01)90268-6

upstream raw materials:

C₄₆H₄₈O₇

2-(1-methylethyl)phenol

thymol

2-Hydroxy-3-isopropylbenzoic acid