1,2-Di-o-acetyl-3-o-benzoyl-5-deoxypentofuranose

Base Information

Chemical Name:1,2-Di-o-acetyl-3-o-benzoyl-5-deoxypentofuranose
CAS No.:4152-81-2
Molecular Formula:C₁₆H₁₈O₇
Molecular Weight:322.315
Hs Code.:
NSC Number:136579
DSSTox Substance ID:DTXSID30961796

Synonyms:4152-81-2;1,2-di-o-acetyl-3-o-benzoyl-5-deoxypentofuranose;NSC136579;DTXSID30961796;NSC-136579

Suppliers and Price of 1,2-Di-o-acetyl-3-o-benzoyl-5-deoxypentofuranose

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 4 raw suppliers

Chemical Property of 1,2-Di-o-acetyl-3-o-benzoyl-5-deoxypentofuranose

Chemical Property:

Vapor Pressure:5.35E-07mmHg at 25°C
Boiling Point:412°C at 760 mmHg
Flash Point:180.5°C
Density:1.27g/cm³
XLogP3:1.9
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:7
Rotatable Bond Count:7
Exact Mass:322.10525291
Heavy Atom Count:23
Complexity:455

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1C(C(C(O1)OC(=O)C)OC(=O)C)OC(=O)C2=CC=CC=C2

Technology Process of 1,2-Di-o-acetyl-3-o-benzoyl-5-deoxypentofuranose

There total 8 articles about 1,2-Di-o-acetyl-3-o-benzoyl-5-deoxypentofuranose which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-xylofuranose

: 4152-80-1,4152-81-2
5-deoxy-3-O-benzoyl-1,2-di(O-acetyl)-β-D-xylofuranose

: 4152-81-2,4152-80-1
5-deoxy-3-O-benzoyl-1,2-di(O-acetyl)-α-D-xylofuranose

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 20 °C

1.2: 0 °C

2.1: triethylamine / tetrahydrofuran / 0 - 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / Reflux

4.1: pyridine / 2 h / 0 - 20 °C

5.1: sulfuric acid; acetic acid / 26 h / 20 °C

With pyridine; lithium aluminium tetrahydride; sulfuric acid; acetic acid; triethylamine; In tetrahydrofuran;
DOI:10.3390/md10040881

Reference yield:

: 532-20-7,613-83-2,7261-25-8,7687-39-0,13221-22-2,14795-83-6,15761-67-8,20074-49-1,25545-03-3,25545-04-4,32445-75-3,34436-17-4,36441-93-7,36468-53-8,37110-85-3,37388-49-1,38029-69-5,40461-77-6,40461-89-0,41546-19-4,41546-20-7,41546-21-8,41546-26-3,41546-29-6,41546-30-9,41546-31-0,126872-16-0,131064-98-7
D-xylofuranose

: 4152-80-1,4152-81-2
5-deoxy-3-O-benzoyl-1,2-di(O-acetyl)-β-D-xylofuranose

: 4152-81-2,4152-80-1
5-deoxy-3-O-benzoyl-1,2-di(O-acetyl)-α-D-xylofuranose

Guidance literature:: Multi-step reaction with 5 steps

1.1: sulfuric acid / 20 °C

1.2: 0 °C

2.1: triethylamine / tetrahydrofuran / 0 - 20 °C

3.1: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / Reflux

4.1: pyridine / 2 h / 0 - 20 °C

5.1: sulfuric acid; acetic acid / 26 h / 20 °C

With pyridine; lithium aluminium tetrahydride; sulfuric acid; acetic acid; triethylamine; In tetrahydrofuran;
DOI:10.3390/md10040881

Reference yield:

: 20031-21-4
1,2-O-isopropylidene-α-D-xylose

: 4152-80-1,4152-81-2
5-deoxy-3-O-benzoyl-1,2-di(O-acetyl)-β-D-xylofuranose

: 4152-81-2,4152-80-1
5-deoxy-3-O-benzoyl-1,2-di(O-acetyl)-α-D-xylofuranose

Guidance literature:: Multi-step reaction with 4 steps

1: triethylamine / tetrahydrofuran / 0 - 20 °C

2: lithium aluminium tetrahydride / tetrahydrofuran / 6 h / Reflux

3: pyridine / 2 h / 0 - 20 °C

4: sulfuric acid; acetic acid / 26 h / 20 °C

With pyridine; lithium aluminium tetrahydride; sulfuric acid; acetic acid; triethylamine; In tetrahydrofuran;
DOI:10.3390/md10040881