4-(7,7-Dioxido-8-phenyl-7-thiabicyclo(4.2.0)oct-1-yl)morpholine

Base Information

• Chemical Name: 4-(7,7-Dioxido-8-phenyl-7-thiabicyclo(4.2.0)oct-1-yl)morpholine
• CAS No.: 19158-30-6
• Molecular Formula: C17H23NO3S
• Molecular Weight: 321.4344
• NSC Number: 162298
• DSSTox Substance ID: DTXSID00940795
• Mol file: 19158-30-6.mol

Synonyms:19158-30-6;4-(7,7-Dioxido-8-phenyl-7-thiabicyclo(4.2.0)oct-1-yl)morpholine;NSC162298;NSC 162298;4-(7,7-Dioxido-8-phenyl-7-thiabicyclo[4.2.0]oct-1-yl)morpholine;DTXSID00940795;NSC-162298;6-morpholino-7-phenyl-8$l^{6}-thiabicyclo[4.2.0]octane 8,8-dioxide;1-(Morpholin-4-yl)-8-phenyl-7lambda~6~-thiabicyclo[4.2.0]octane-7,7-dione

Chemical Property of 4-(7,7-Dioxido-8-phenyl-7-thiabicyclo(4.2.0)oct-1-yl)morpholine

Chemical Property:

• Vapor Pressure: 1.02E-10mmHg at 25°C
• Boiling Point: 515°C at 760 mmHg
• Flash Point: 265.3°C
• Density: 1.282g/cm³
• XLogP3: 1.7
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 4
• Rotatable Bond Count: 2
• Exact Mass: 321.13986477
• Heavy Atom Count: 22
• Complexity: 503

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CCC2(C(C1)S(=O)(=O)C2C3=CC=CC=C3)N4CCOCC4

Technology Process of 4-(7,7-Dioxido-8-phenyl-7-thiabicyclo(4.2.0)oct-1-yl)morpholine

There total 4 articles about 4-(7,7-Dioxido-8-phenyl-7-thiabicyclo(4.2.0)oct-1-yl)morpholine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

4-cyclohexen-1-ylmorpholine (670-80-4) + phenylmethylsulphonyl fluoride (329-98-6) → 1-Morpholino-8-phenyl-7-thia-bicyclo<4.2.0>octan-7,7-dioxid (19158-30-6,56942-87-1)

Guidance literature:

With triphenyl(phenylmethylene)phosphorane;

DOI:10.1021/jo00932a013

Reference yield:

→ 1-Morpholino-8-phenyl-7-thia-bicyclo<4.2.0>octan-7,7-dioxid (19158-30-6,56942-87-1)

Guidance literature:

Phenylsulfen in Ae., 1-Morpholino-cyclohexen;

DOI:10.1039/j39680001612

Reference yield:

→ 4-(7,7-dioxo-8-phenyl-7λ6-thia-bicyclo[4.2.0]oct-1-yl)-morpholine (19158-30-6,56942-86-0,56942-87-1)

Guidance literature:

Phenyldiazomethan, SO2, 1-Morpholinocyclohexen;

upstream raw materials:

4-cyclohexen-1-ylmorpholine

phenylmethylsulphonyl fluoride