Adenosine, N-[(4-nitrophenyl)methyl]-, 2',3',5'-triacetate

Base Information

Chemical Name:Adenosine, N-[(4-nitrophenyl)methyl]-, 2',3',5'-triacetate
CAS No.:112533-71-8
Molecular Formula:C23H24N6O9
Molecular Weight:528.478
Hs Code.:

Synonyms:

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Chemical Property of Adenosine, N-[(4-nitrophenyl)methyl]-, 2',3',5'-triacetate

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Technology Process of Adenosine, N-[(4-nitrophenyl)methyl]-, 2',3',5'-triacetate

There total 1 articles about Adenosine, N-[(4-nitrophenyl)methyl]-, 2',3',5'-triacetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 40297-54-9
N6-(p-Nirobenzyl)adenosine

: 108-24-7
acetic anhydride

: 112533-71-8
Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-(4-nitro-benzylamino)-purin-9-yl]-tetrahydro-furan-3-yl ester

Guidance literature:: In pyridine; for 3h; Ambient temperature;
DOI:10.1021/jm00399a010

Reference yield:

: 112533-71-8
Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-(4-nitro-benzylamino)-purin-9-yl]-tetrahydro-furan-3-yl ester

: 98866-49-0
N-[(4-amino-3-iodophenyl)methyl]-Adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 1.) hydrogen, 2.) ammonia / 1.) 5percent Pd/C / 1.) methanol, 40 psi, 4 h, 2.) 1.5 h

2: 5.3 percent / iodine, aq. HCl / ethanol / 24 h / Ambient temperature

With hydrogenchloride; ammonia; hydrogen; iodine; palladium on activated charcoal; In ethanol;
DOI:10.1021/jm00399a010

Reference yield:

: 112533-71-8
Acetic acid (2R,3R,4R,5R)-4-acetoxy-5-acetoxymethyl-2-[6-(4-nitro-benzylamino)-purin-9-yl]-tetrahydro-furan-3-yl ester

: 95523-13-0
[125I]-N₆-(4-Aminobenzyl)adenosine

Guidance literature:: With ammonia; hydrogen; palladium on activated charcoal; Yield given. Multistep reaction; 1.) methanol, 40 psi, 4 h, 2.) 1.5 h;
DOI:10.1021/jm00399a010