2,3,4,5-Tetra-o-acetyl-1-deoxy-1-({4,5-dimethyl-2-[(e)-(4-nitrophenyl)diazenyl]phenyl}amino)pentitol

Base Information

• Chemical Name: 2,3,4,5-Tetra-o-acetyl-1-deoxy-1-({4,5-dimethyl-2-[(e)-(4-nitrophenyl)diazenyl]phenyl}amino)pentitol
• CAS No.: 6973-44-0
• Molecular Formula: C₂₇H₃₂N₄O₁₀
• Molecular Weight: 572.572
• NSC Number: 41824
• DSSTox Substance ID: DTXSID00285431

Synonyms:6973-44-0;NSC41824;2,3,4,5-tetra-o-acetyl-1-deoxy-1-({4,5-dimethyl-2-[(e)-(4-nitrophenyl)diazenyl]phenyl}amino)pentitol;DTXSID00285431;NSC-41824

Chemical Property of 2,3,4,5-Tetra-o-acetyl-1-deoxy-1-({4,5-dimethyl-2-[(e)-(4-nitrophenyl)diazenyl]phenyl}amino)pentitol

Chemical Property:

• Vapor Pressure: 3.25E-18mmHg at 25°C
• Boiling Point: 677.5°Cat760mmHg
• Flash Point: 363.6°C
• Density: 1.3g/cm³
• XLogP3: 4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 13
• Rotatable Bond Count: 16
• Exact Mass: 572.21184323
• Heavy Atom Count: 41
• Complexity: 947

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: CC1=CC(=C(C=C1C)N=NC2=CC=C(C=C2)[N+](=O)[O-])NCC(C(C(COC(=O)C)OC(=O)C)OC(=O)C)OC(=O)C

Technology Process of 2,3,4,5-Tetra-o-acetyl-1-deoxy-1-({4,5-dimethyl-2-[(e)-(4-nitrophenyl)diazenyl]phenyl}amino)pentitol

There total 1 articles about 2,3,4,5-Tetra-o-acetyl-1-deoxy-1-({4,5-dimethyl-2-[(e)-(4-nitrophenyl)diazenyl]phenyl}amino)pentitol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

p-nitrobenzenediazonium (14368-49-1) + L-ribo-5-(3.4-dimethyl-anilino)-1.2.3.4-tetraacetoxy-pentane (911650-71-0) → 1-[6-(4-nitro-phenylazo)-3.4-dimethyl-anilino]-tetra-O-acetyl-D-1-deoxy-ribitol (6973-44-0) + 1-[2-(4-nitro-phenylazo)-3.4-dimethyl-anilino]-tetra-O-acetyl-D-1-deoxy-ribitol

Guidance literature:

DOI:10.1021/ja01198a068

Reference yield:

1-[6-(4-nitro-phenylazo)-3.4-dimethyl-anilino]-tetra-O-acetyl-D-1-deoxy-ribitol (6973-44-0) → 1-[6-(4-nitro-phenylazo)-3.4-dimethyl-anilino]-D-1-deoxy-ribitol (1194734-29-6)

Guidance literature:

With methanol; sodium methylate;

DOI:10.1021/ja01198a068

upstream raw materials:

p-nitrobenzenediazonium

L-ribo-5-(3.4-dimethyl-anilino)-1.2.3.4-tetraacetoxy-pentane

Downstream raw materials:

1-[6-(4-nitro-phenylazo)-3.4-dimethyl-anilino]-D-1-deoxy-ribitol

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