5H-DIBENZO(a,d)CYCLOHEPTENE-4-ETHYLAMINE, 10,11-DIHYDRO-5-METHYLENE-

Base Information

Chemical Name:5H-DIBENZO(a,d)CYCLOHEPTENE-4-ETHYLAMINE, 10,11-DIHYDRO-5-METHYLENE-
CAS No.:36065-48-2
Molecular Formula:C18H19N
Molecular Weight:249.3502
Hs Code.:
DSSTox Substance ID:DTXSID60189643
Nikkaji Number:J42.169C
Wikidata:Q83061822
Mol file:36065-48-2.mol

Synonyms:BRN 2943961;36065-48-2;5H-DIBENZO(a,d)CYCLOHEPTENE-4-ETHYLAMINE, 10,11-DIHYDRO-5-METHYLENE-;10,11-Dihydro-5-methylene-5H-dibenzo(a,d)cycloheptene-4-ethylamine;DTXSID60189643;LS-60722;10,11-Dihydro-5-methylene-5H-dibenzo[a,d]cycloheptene-4-ethanamine;5H-Dibenzo[a,d]cycloheptene-4-ethanamine, 10,11-dihydro-5-methylene-

Suppliers and Price of 5H-DIBENZO(a,d)CYCLOHEPTENE-4-ETHYLAMINE, 10,11-DIHYDRO-5-METHYLENE-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of 5H-DIBENZO(a,d)CYCLOHEPTENE-4-ETHYLAMINE, 10,11-DIHYDRO-5-METHYLENE-

Chemical Property:

Vapor Pressure:1.09E-06mmHg at 25°C
Boiling Point:402.5°Cat760mmHg
Flash Point:193.8°C
PSA：26.02000
Density:1.09g/cm³
LogP:4.04820
XLogP3:3.6
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:2
Exact Mass:249.151749610
Heavy Atom Count:19
Complexity:322

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C=C1C2=CC=CC=C2CCC3=C1C(=CC=C3)CCN

Technology Process of 5H-DIBENZO(a,d)CYCLOHEPTENE-4-ETHYLAMINE, 10,11-DIHYDRO-5-METHYLENE-

There total 5 articles about 5H-DIBENZO(a,d)CYCLOHEPTENE-4-ETHYLAMINE, 10,11-DIHYDRO-5-METHYLENE- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 36065-52-8
10,11-Dihydro-5-methylen-5H-dibenzocyclohepten-4-acetonitril

: 36065-48-2
2'-<10,11-Dihydro-5-methylen-5H-dibenzocyclohepten-4>-aethylamin

Guidance literature:: With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether;
DOI:10.1021/jm00292a024

Reference yield:

: 36065-51-7
10,11-Dihydro-5-methylen-5H-dibenzocyclohepten-4-methylchlorid

: 36065-48-2
2'-<10,11-Dihydro-5-methylen-5H-dibenzocyclohepten-4>-aethylamin

Guidance literature:: Multi-step reaction with 2 steps

1: dimethylformamide; H₂O

2: LiAlH₄, AlCl₃ / diethyl ether

With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; water; N,N-dimethyl-formamide;
DOI:10.1021/jm00292a024

Reference yield:

: 33953-64-9
10,11-Dihydro-N,N-dimethyl-5-methylen-5H-dibenzocyclohepten-4-methylamin

: 36065-48-2
2'-<10,11-Dihydro-5-methylen-5H-dibenzocyclohepten-4>-aethylamin

Guidance literature:: Multi-step reaction with 3 steps

1: ClCO₂Et / benzene

2: dimethylformamide; H₂O

3: LiAlH₄, AlCl₃ / diethyl ether

With lithium aluminium tetrahydride; aluminium trichloride; chloroformic acid ethyl ester; In diethyl ether; water; N,N-dimethyl-formamide; benzene;
DOI:10.1021/jm00292a024