Dibenzoylmethane monoxime

Base Information

• Chemical Name: Dibenzoylmethane monoxime
• CAS No.: 5741-75-3
• Molecular Formula: C₁₅H₁₃NO₂
• Molecular Weight: 239.274
• UNII: 4WWW59D42P
• Mol file: 5741-75-3.mol

Synonyms:Dibenzoylmethane monoxime;Dibenzoylmethane monoxime [MI];4WWW59D42P;NSC-106655;UNII-4WWW59D42P;1,3-Propanedione, 1,3-diphenyl-, oxime;5741-75-3

Chemical Property of Dibenzoylmethane monoxime

Chemical Property:

• Vapor Pressure: 4.88E-08mmHg at 25°C
• Boiling Point: °Cat760mmHg
• Flash Point: °C
• Density: 1.448g/cm³
• XLogP3: 3.4
• Hydrogen Bond Donor Count: 1
• Hydrogen Bond Acceptor Count: 3
• Rotatable Bond Count: 4
• Exact Mass: 239.094628657
• Heavy Atom Count: 18
• Complexity: 300

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1=CC=C(C=C1)C(=NO)CC(=O)C2=CC=CC=C2
• Isomeric SMILES: C1=CC=C(C=C1)/C(=N/O)/CC(=O)C2=CC=CC=C2

Technology Process of Dibenzoylmethane monoxime

There total 6 articles about Dibenzoylmethane monoxime which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1-nitro-1-phenylcyclopropane (79863-09-5) → dibenzoylmethane monooxime (5741-75-3)

Guidance literature:

With acetic acid; at 0 ℃;

Reference yield:

(Z)-3-ethoxy-1,3-diphenylprop-2-en-1-one (1907-69-3) → dibenzoylmethane monooxime (5741-75-3)

Guidance literature:

With ethanol; hydroxylamine;

Reference yield:

1,3-diphenylpropanedione (120-46-7,61346-73-4) → dibenzoylmethane monooxime (5741-75-3)

Guidance literature:

With ethanol; hydroxylamine;

upstream raw materials:

(Z)-3-ethoxy-1,3-diphenylprop-2-en-1-one

1,3-diphenylpropanedione

1,3-diphenyl-propen-3-one

1-nitro-1-phenylcyclopropane

Downstream raw materials:

3,5-diphehylisoxazole

erythro-3-amino-1,3-diphenylpropanol

Refernces