9-Fluoro-5,11-dimethyl-6H-pyrido[4,3-b]carbazole

Base Information

Chemical Name:9-Fluoro-5,11-dimethyl-6H-pyrido[4,3-b]carbazole
CAS No.:69467-92-1
Molecular Formula:C₁₇H₁₃FN₂
Molecular Weight:264.302
Hs Code.:
NSC Number:611401

Synonyms:9-Fluoro-5,11-dimethyl-6H-pyrido[4,3-b]carbazole;NSC611401;9-Fluoroellipticine;9-Fluoro-5,11-dimethyl-6H-pyrido(4,3-b)carbazole;6H-Pyrido(4,3-b)carbazole, 5,11-dimethyl-9-fluoro-;NSC-611401;69467-92-1

Suppliers and Price of 9-Fluoro-5,11-dimethyl-6H-pyrido[4,3-b]carbazole

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 9-Fluoro-5,11-dimethyl-6H-pyrido[4,3-b]carbazole

Chemical Property:

Vapor Pressure:1.44E-09mmHg at 25°C
Boiling Point:498.1°Cat760mmHg
Flash Point:255°C
Density:1.32g/cm³
XLogP3:4.9
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:264.10627659
Heavy Atom Count:20
Complexity:374

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:

Useful:

Canonical SMILES:CC1=C2C=CN=CC2=C(C3=C1NC4=C3C=C(C=C4)F)C

Technology Process of 9-Fluoro-5,11-dimethyl-6H-pyrido[4,3-b]carbazole

There total 9 articles about 9-Fluoro-5,11-dimethyl-6H-pyrido[4,3-b]carbazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 917-54-4
methyllithium

: 3-fluoroindolo[1,2-b][2,7]naphthyridine-6,11-quinone

: 69467-92-1
9-fluoroellipticine

Guidance literature:: methyllithium; 3-fluoroindolo[1,2-b][2,7]naphthyridine-6,11-quinone; In tetrahydrofuran; diethyl ether; at -110 - 20 ℃; for 16h;

With sodium tetrahydroborate; In ethanol; for 18h; Reflux;
DOI:10.3987/COM-18-S(T)30

Reference yield:

: 553-94-6
4-bromo-m-xylene

: 69467-92-1
9-fluoroellipticine

Guidance literature:: Multi-step reaction with 7 steps

1: 30 percent / copper bronze, K₂CO₃ / 19 h / 200 °C

2: 10 percent / ethanol / 26 h / Irradiation

3: 83 percent / phosphorus oxychloride / trichloroethene / 3.5 h / Heating

4: 2 h / Heating

5: H₂ / Adams catalyst / ethanol / Ambient temperature

6: pyridine / 96 h / Ambient temperature

7: 27 mg / aq. HCl / dioxane / 7.5 h / Heating

With pyridine; hydrogenchloride; hydrogen; copper; potassium carbonate; trichlorophosphate; platinum(IV) oxide; In 1,4-dioxane; ethanol; Trichloroethylene;

Reference yield:

: 727-31-1
N-(4-fluorophenyl)-4-methylbenzenesulfonamide

: 69467-92-1
9-fluoroellipticine

Guidance literature:: Multi-step reaction with 7 steps

1: 30 percent / copper bronze, K₂CO₃ / 19 h / 200 °C

2: 10 percent / ethanol / 26 h / Irradiation

3: 83 percent / phosphorus oxychloride / trichloroethene / 3.5 h / Heating

4: 2 h / Heating

5: H₂ / Adams catalyst / ethanol / Ambient temperature

6: pyridine / 96 h / Ambient temperature

7: 27 mg / aq. HCl / dioxane / 7.5 h / Heating

With pyridine; hydrogenchloride; hydrogen; copper; potassium carbonate; trichlorophosphate; platinum(IV) oxide; In 1,4-dioxane; ethanol; Trichloroethylene;