2H-Benzimidazol-2-one, 1,3-dihydro-6-bromo-1-phenyl-

Base Information

Chemical Name:2H-Benzimidazol-2-one, 1,3-dihydro-6-bromo-1-phenyl-
CAS No.:79759-42-5
Molecular Formula:C13H9BrN2O
Molecular Weight:289.131
Hs Code.:
DSSTox Substance ID:DTXSID30229868
Wikidata:Q83110235

Synonyms:BRN 5543659;2H-Benzimidazol-2-one, 1,3-dihydro-6-bromo-1-phenyl-;1,3-Dihydro-6-bromo-1-phenyl-2H-benzimidazol-2-one;C13H9BrN2O;79759-42-5;C13-H9-Br-N2-O;SCHEMBL15396404;DTXSID30229868;LS-33285

Suppliers and Price of 2H-Benzimidazol-2-one, 1,3-dihydro-6-bromo-1-phenyl-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

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Total 0 raw suppliers

Chemical Property of 2H-Benzimidazol-2-one, 1,3-dihydro-6-bromo-1-phenyl-

Chemical Property:

Boiling Point:°Cat760mmHg
Flash Point:°C
Density:1.584g/cm³
XLogP3:3
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:1
Rotatable Bond Count:1
Exact Mass:287.98983
Heavy Atom Count:17
Complexity:304

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1=CC=C(C=C1)N2C3=C(C=CC(=C3)Br)NC2=O

Technology Process of 2H-Benzimidazol-2-one, 1,3-dihydro-6-bromo-1-phenyl-

There total 9 articles about 2H-Benzimidazol-2-one, 1,3-dihydro-6-bromo-1-phenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.2%

: 79759-16-3
(4-Bromo-2-phenylamino-phenyl)-carbamic acid ethyl ester

: 79759-42-5
6-bromo-1-phenyl-1H-benzo[d]imidazol-2(3H)-one

Guidance literature:: With sodium ethanolate; In ethanol; for 4h; Inert atmosphere; Reflux;

Reference yield: 78.0%

: 79759-42-5
6-bromo-1-phenyl-1H-benzo[d]imidazol-2(3H)-one

Guidance literature:: With triethylamine; In dichloromethane; at 0 ℃; for 1h; Inert atmosphere;

Reference yield:

: 321-23-3
4-bromo-2-fluoronitrobenzene

: 79759-42-5
6-bromo-1-phenyl-1H-benzo[d]imidazol-2(3H)-one

Guidance literature:: Multi-step reaction with 4 steps

1: dimethyl sulfoxide / 18 h / Inert atmosphere; Reflux

2: zinc; acetic acid / ethanol; water / 2 h / 0 - 20 °C / Inert atmosphere

3: triethylamine / chloroform / 2 h / 0 - 20 °C / Inert atmosphere

4: sodium ethanolate / ethanol / 4 h / Inert atmosphere; Reflux

With sodium ethanolate; acetic acid; triethylamine; zinc; In ethanol; chloroform; water; dimethyl sulfoxide;