1,3-BENZODIOXOLE-5-CARBOXAMIDE, N-[[4-(PHENYLMETHYL)-2-MORPHOLINYL]METHYL]-

Base Information

Chemical Name:1,3-BENZODIOXOLE-5-CARBOXAMIDE, N-[[4-(PHENYLMETHYL)-2-MORPHOLINYL]METHYL]-
CAS No.:112885-38-8
Molecular Formula:C20H22N2O4
Molecular Weight:354.40000
Hs Code.:
Mol file:112885-38-8.mol

Synonyms:3,4-dioxymethylene mandelic acid;

Suppliers and Price of 1,3-BENZODIOXOLE-5-CARBOXAMIDE, N-[[4-(PHENYLMETHYL)-2-MORPHOLINYL]METHYL]-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

American Custom Chemicals Corporation
N-[[4-(PHENYLMETHYL)-2-MORPHOLINYL]METHYL]-1,3-BENZODIOXOLE-5-CARBOXAMIDE 95.00%
5MG
$ 503.09

Total 2 raw suppliers

Chemical Property of 1,3-BENZODIOXOLE-5-CARBOXAMIDE, N-[[4-(PHENYLMETHYL)-2-MORPHOLINYL]METHYL]-

Chemical Property:

Vapor Pressure:1.76E-10mmHg at 25°C
Boiling Point:509oC at 760 mmHg
Flash Point:261.6oC
PSA：63.52000
Density:1.248g/cm3
LogP:2.55880

Purity/Quality:

99% ^*data from raw suppliers

N-[[4-(PHENYLMETHYL)-2-MORPHOLINYL]METHYL]-1,3-BENZODIOXOLE-5-CARBOXAMIDE 95.00% ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 1,3-BENZODIOXOLE-5-CARBOXAMIDE, N-[[4-(PHENYLMETHYL)-2-MORPHOLINYL]METHYL]-

There total 10 articles about 1,3-BENZODIOXOLE-5-CARBOXAMIDE, N-[[4-(PHENYLMETHYL)-2-MORPHOLINYL]METHYL]- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 94-53-1
Piperonylic acid

: 110859-47-7,140646-11-3
(4-benzylmorpholin-2-yl)methanamine

: 110-17-8,26099-09-2
(2E)-but-2-enedioic acid

: 112885-38-8
N-<(4-benzyl-2-morpholinyl)methyl>-3,4-(methylenedioxy)benzamide

Guidance literature:: With thionyl chloride; triethylamine; In N-methyl-acetamide; chloroform;

Reference yield:

: 147767-51-9,126645-52-1
4-benzyl-2-cyanomorpholine

: 112885-38-8
N-<(4-benzyl-2-morpholinyl)methyl>-3,4-(methylenedioxy)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) H₂, acetic acid / 1.) Raney nickel / 1.) 95 percent EtOH, RT, 2.) CHCl₃, RT, 2 h

2: 100 percent / 10percent HCl / 4 h / Heating

3: triethylamine / CHCl₃ / Ambient temperature

With hydrogenchloride; hydrogen; acetic acid; triethylamine; nickel; In chloroform;
DOI:10.1021/jm00167a020

Reference yield:

: 104-63-2
N-Benzylethanolamine

: 112885-38-8
N-<(4-benzyl-2-morpholinyl)methyl>-3,4-(methylenedioxy)benzamide

Guidance literature:: Multi-step reaction with 3 steps

1: 3 h / 80 °C

2: concd. H₂SO₄ / 1 h / 150 °C

3: triethylamine / CHCl₃ / Ambient temperature

With sulfuric acid; triethylamine; In chloroform;
DOI:10.1021/jm00167a020