5H-Indeno[1,2-c]pyridin-5-yl, 1,3,4,6,7,8,9-heptachloro-5-(pentachlorophenyl)-

Base Information

• Chemical Name: 5H-Indeno[1,2-c]pyridin-5-yl, 1,3,4,6,7,8,9-heptachloro-5-(pentachlorophenyl)-
• CAS No.: 112988-79-1
• Molecular Formula: C₁₈Cl₁₂N
• Molecular Weight: 655.641
• Mol file: 112988-79-1.mol

Synonyms:

Chemical Property of 5H-Indeno[1,2-c]pyridin-5-yl, 1,3,4,6,7,8,9-heptachloro-5-(pentachlorophenyl)-

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 5H-Indeno[1,2-c]pyridin-5-yl, 1,3,4,6,7,8,9-heptachloro-5-(pentachlorophenyl)-

There total 3 articles about 5H-Indeno[1,2-c]pyridin-5-yl, 1,3,4,6,7,8,9-heptachloro-5-(pentachlorophenyl)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

diphenyl(tetrachloro-4-pyridyl)methanol (30718-16-2) → perchloro-3-aza-9-phenylfluorenyl radical (112988-79-1)

Guidance literature:

Multi-step reaction with 4 steps

1: 100 percent / 57percent aq. HI / hexane / 4 h / Heating

2: 75 percent / S₂Cl₂, SO₂Cl₂, AlCl₃ / 7 h / Heating

3: 1.) NaOH, Me₂SO, 2.) I₂ / 1.) ethyl ether, 6 d, 2.) ethyl ether, 23 h

4: 11 percent / 1 h / 295 - 300 °C

With disulfur dichloride; sodium hydroxide; aluminium trichloride; sulfuryl dichloride; hydrogen iodide; iodine; dimethyl sulfoxide; In hexane;

DOI:10.1021/jo00241a026

Reference yield:

diphenyl(tetrachloro-4-pyridyl)methane (105150-43-4) → perchloro-3-aza-9-phenylfluorenyl radical (112988-79-1)

Guidance literature:

Multi-step reaction with 3 steps

1: 75 percent / S₂Cl₂, SO₂Cl₂, AlCl₃ / 7 h / Heating

2: 1.) NaOH, Me₂SO, 2.) I₂ / 1.) ethyl ether, 6 d, 2.) ethyl ether, 23 h

3: 11 percent / 1 h / 295 - 300 °C

With disulfur dichloride; sodium hydroxide; aluminium trichloride; sulfuryl dichloride; iodine; dimethyl sulfoxide;

DOI:10.1021/jo00241a026

Reference yield:

αH-tetradecachlorodiphenyl(4-pyridyl)methane (105165-33-1) → perchloro-3-aza-9-phenylfluorenyl radical (112988-79-1)

Guidance literature:

Multi-step reaction with 2 steps

1: 1.) NaOH, Me₂SO, 2.) I₂ / 1.) ethyl ether, 6 d, 2.) ethyl ether, 23 h

2: 11 percent / 1 h / 295 - 300 °C

With sodium hydroxide; iodine; dimethyl sulfoxide;

DOI:10.1021/jo00241a026

upstream raw materials:

diphenyl(tetrachloro-4-pyridyl)methanol

diphenyl(tetrachloro-4-pyridyl)methane

αH-tetradecachlorodiphenyl(4-pyridyl)methane