3'-Thymidylic acid, mono(2-chlorophenyl) ester, 5'-[2-chlorophenyl 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl phosphate], compd. with N,N-diethylethanamine (1:1)

Base Information

Chemical Name:3'-Thymidylic acid, mono(2-chlorophenyl) ester, 5'-[2-chlorophenyl 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl phosphate], compd. with N,N-diethylethanamine (1:1)
CAS No.:113019-19-5
Molecular Formula:C₆H₁₅N*C₄₄H₄₃Cl₂N₃O₁₂P₂
Molecular Weight:1039.88
Hs Code.:

3'-Thymidylic acid, mono(2-chlorophenyl) ester, 5'-[2-chlorophenyl
2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl phosphate], compd.
with N,N-diethylethanamine (1:1)

Synonyms:

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Chemical Property of 3'-Thymidylic acid, mono(2-chlorophenyl) ester, 5'-[2-chlorophenyl 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl phosphate], compd. with N,N-diethylethanamine (1:1)

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Technology Process of 3'-Thymidylic acid, mono(2-chlorophenyl) ester, 5'-[2-chlorophenyl 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl phosphate], compd. with N,N-diethylethanamine (1:1)

There total 3 articles about 3'-Thymidylic acid, mono(2-chlorophenyl) ester, 5'-[2-chlorophenyl 2-[[(4-methoxyphenyl)diphenylmethyl]amino]ethyl phosphate], compd. with N,N-diethylethanamine (1:1) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 113019-15-1
Phosphoric acid 2-chloro-phenyl ester 2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethyl ester; compound with pyridine

: 113019-19-5
Phosphoric acid (2R,3S,5R)-2-[(2-chloro-phenoxy)-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethoxy)-phosphoryloxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / 1-(mesitylenesulfonyl)-3-nitro-1,2,4-triazole, 1-methyl-imidazole / Ambient temperature

2: pyridine; H₂O / 0.17 h / Ambient temperature

With 1-methyl-1H-imidazole; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In pyridine; water;
DOI:10.1016/S0040-4039(00)96161-6

Reference yield:

: 80817-40-9
2'-deoxythymidine-3'-O-(2-chlorophenyl-2-cyanoethyl)phosphate

: 113019-19-5
Phosphoric acid (2R,3S,5R)-2-[(2-chloro-phenoxy)-(2-{[(4-methoxy-phenyl)-diphenyl-methyl]-amino}-ethoxy)-phosphoryloxymethyl]-5-(5-methyl-2,4-dioxo-3,4-dihydro-2H-pyrimidin-1-yl)-tetrahydro-furan-3-yl ester 2-chloro-phenyl ester; compound with triethyl-amine

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / 1-(mesitylenesulfonyl)-3-nitro-1,2,4-triazole, 1-methyl-imidazole / Ambient temperature

2: pyridine; H₂O / 0.17 h / Ambient temperature

With 1-methyl-1H-imidazole; 1-(mesitylene-2-sulfonyl)-3-nitro-1H-1,2,4-triazole; In pyridine; water;
DOI:10.1016/S0040-4039(00)96161-6