Cholest-7-en-6-one, 2,3,14-trihydroxy-, (2beta,3beta,5beta)-

Base Information

Chemical Name:Cholest-7-en-6-one, 2,3,14-trihydroxy-, (2beta,3beta,5beta)-
CAS No.:7698-69-3
Molecular Formula:C₂₇H₄₄O₄
Molecular Weight:432.644
Hs Code.:
Nikkaji Number:J144.031D
Mol file:7698-69-3.mol

Synonyms:7698-69-3;22,25-Bisdeoxyecdysone;22,25-Deoxy-alpha-ecdysone;(2beta,3beta,5beta)-2,3,14-Trihydroxycholest-7-en-6-one;2beta,3beta,14alpha-trihydroxy-5beta-cholest-7-en-6-one;Cholest-7-en-6-one, 2,3,14-trihydroxy-, (2beta,3beta,5beta)-

Suppliers and Price of Cholest-7-en-6-one, 2,3,14-trihydroxy-, (2beta,3beta,5beta)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 3 raw suppliers

Chemical Property of Cholest-7-en-6-one, 2,3,14-trihydroxy-, (2beta,3beta,5beta)-

Chemical Property:

Vapor Pressure:4.71E-15mmHg at 25°C
Boiling Point:563.7°Cat760mmHg
Flash Point:308.8°C
PSA：253.00000
Density:1.12g/cm³
LogP:9.15040
XLogP3:4.6
Hydrogen Bond Donor Count:3
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:5
Exact Mass:432.32395988
Heavy Atom Count:31
Complexity:744

Purity/Quality:

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC(C)CCCC(C)C1CCC2(C1(CCC3C2=CC(=O)C4C3(CC(C(C4)O)O)C)C)O
Isomeric SMILES:C[C@H](CCCC(C)C)[C@H]1CC[C@@]2([C@@]1(CC[C@H]3C2=CC(=O)[C@H]4[C@@]3(C[C@@H]([C@@H](C4)O)O)C)C)O

Technology Process of Cholest-7-en-6-one, 2,3,14-trihydroxy-, (2beta,3beta,5beta)-

There total 13 articles about Cholest-7-en-6-one, 2,3,14-trihydroxy-, (2beta,3beta,5beta)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 40.0%

: 7698-68-2
2β,3β-diacetoxy-14α-hydroxy-5α-chloest-7-en-6-one

: 7698-67-1
5α-22,25-dideoxy-ecdysone

: 7698-69-3
22,25-Dideoxyecdysone

Guidance literature:: With potassium carbonate; In methanol; water; at 45 - 50 ℃; for 0.416667h;
DOI:10.1023/A:1021673924353

Reference yield:

: 7698-66-0
2β,3β-diacetoxy-5α-cholest-7-en-6-one

: 7698-69-3
22,25-Dideoxyecdysone

Guidance literature:: Multi-step reaction with 2 steps

1: 89 percent / SeO₂ / dioxane / 0.58 h / 81 - 85 °C

2: 40 percent / K₂CO₃ / methanol; H₂O / 0.42 h / 45 - 50 °C

With selenium(IV) oxide; potassium carbonate; In 1,4-dioxane; methanol; water;
DOI:10.1023/A:1021673924353

Reference yield:

: 7703-80-2
2β,3β-Diacetoxy-5α-cholestan-6-one

: 7698-69-3
22,25-Dideoxyecdysone

Guidance literature:: Multi-step reaction with 4 steps

1: Br₂, AcOH / diethyl ether

2: Li₂CO₃ / dimethylformamide

3: aq. K₂CO₃ / methanol

4: SeO₂

With selenium(IV) oxide; bromine; lithium carbonate; potassium carbonate; acetic acid; In methanol; diethyl ether; N,N-dimethyl-formamide;
DOI:10.1016/S0039-128X(70)80099-X