Technology Process of 2H-1-Benzopyran-2-one, 3-(2-[1,1'-biphenyl]-4-ylethenyl)-
There total 5 articles about 2H-1-Benzopyran-2-one, 3-(2-[1,1'-biphenyl]-4-ylethenyl)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
toluene-4-sulfonic acid; acetic acid;
for 3h;
Heating;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 76 percent / NaOAc, Ac2O
2: 66 percent / 30percent conc. HCl, glacial acetic acid / 5 h / Heating
3: 78 percent / NaBH4 / tetrahydrofuran / 1 h / Ambient temperature
4: 70 percent / p-toluenesulphonic acid, glacial acetic acid / 3 h / Heating
With
hydrogenchloride; sodium tetrahydroborate; sodium acetate; acetic anhydride; toluene-4-sulfonic acid; acetic acid;
In
tetrahydrofuran;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 76 percent / NaOAc, Ac2O
2: 66 percent / 30percent conc. HCl, glacial acetic acid / 5 h / Heating
3: 78 percent / NaBH4 / tetrahydrofuran / 1 h / Ambient temperature
4: 70 percent / p-toluenesulphonic acid, glacial acetic acid / 3 h / Heating
With
hydrogenchloride; sodium tetrahydroborate; sodium acetate; acetic anhydride; toluene-4-sulfonic acid; acetic acid;
In
tetrahydrofuran;