4-(dimethylamino)benzaldehyde 5H-[1,2,4]triazino[5,6-b]indol-3-ylhydrazone

Base Information

• Chemical Name: 4-(dimethylamino)benzaldehyde 5H-[1,2,4]triazino[5,6-b]indol-3-ylhydrazone
• CAS No.: 113306-11-9
• Molecular Formula: C₁₈H₁₇N₇
• Molecular Weight: 331.38
• Mol file: 113306-11-9.mol

Synonyms:3-(p)-dimethylaminobenzalhydrazino-1,2,4-triazino[5,6-b]indole;Dimethyl-{4-[(5H-[1,2,4]triazino[5,6-b]indol-3-yl)-hydrazonomethyl]-phenyl}-amine;

Chemical Property of 4-(dimethylamino)benzaldehyde 5H-[1,2,4]triazino[5,6-b]indol-3-ylhydrazone

Chemical Property:

• PSA: 82.09000
• LogP: 3.09110

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 4-(dimethylamino)benzaldehyde 5H-[1,2,4]triazino[5,6-b]indol-3-ylhydrazone

There total 2 articles about 4-(dimethylamino)benzaldehyde 5H-[1,2,4]triazino[5,6-b]indol-3-ylhydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

3-hydrazino-5H-[1,2,4]triazino[5,6-b]indole (31523-22-5) + 4-dimethylamino-benzaldehyde (100-10-7) → 3-(p)-dimethylaminobenzalhydrazino-1,2,4-triazino<5,6-b>indole (113306-11-9)

Guidance literature:

In ethanol; for 2.5h; Heating;

DOI:10.1002/jhet.5570240542

Reference yield:

2,5-dihydro-3H-1,2,4-triazino[5,6-b]indole-3-thione (28668-95-3) → 3-(p)-dimethylaminobenzalhydrazino-1,2,4-triazino<5,6-b>indole (113306-11-9)

Guidance literature:

Multi-step reaction with 2 steps

1: hydrazine / ethanol / Heating

2: 75 percent / ethanol / 2.5 h / Heating

With hydrazine; In ethanol;

DOI:10.1002/jhet.5570240542

Reference yield: 38.0%

3-(p)-dimethylaminobenzalhydrazino-1,2,4-triazino<5,6-b>indole (113306-11-9) → 3-(p)-dimethylaminophenyl-1,2,4-triazolo<4,3-b>triazino<7,6-b>indole (113306-14-2)

Guidance literature:

With bromine; In acetic acid; for 5h; Ambient temperature;

DOI:10.1002/jhet.5570240542

upstream raw materials:

3-hydrazino-5H-[1,2,4]triazino[5,6-b]indole

4-dimethylamino-benzaldehyde

2,5-dihydro-3H-1,2,4-triazino[5,6-b]indole-3-thione

Downstream raw materials:

3-(p)-dimethylaminophenyl-1,2,4-triazolo<4,3-b>triazino<7,6-b>indole

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