Technology Process of Benzyl(ethyl)dimethylgermane
There total 1 articles about Benzyl(ethyl)dimethylgermane which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
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With
C2H5MgBr;
In
diethyl ether;
Ethylation of reaction mixture with EtMgBr in Et2O at 0°C with stirring for 0.5 h, then stirring of the mixture at room temp. for 1 h under Ar.; addn. of H2O and NH4Cl, sepn. of phases, extn. of aq. phase (Et2O), removal of solvent, pptn. of tetraphenylnaphthalene (pentane), investigation of crude products by GC-MS anal.;