6-[(11R)-11-hydroxydodecyl]-3-methoxy-2-methyl-1H-pyridin-4-one

Base Information

Chemical Name:6-[(11R)-11-hydroxydodecyl]-3-methoxy-2-methyl-1H-pyridin-4-one
CAS No.:70001-21-7
Molecular Formula:C₁₉H₃₃NO₃
Molecular Weight:323.476
Hs Code.:
Mol file:70001-21-7.mol

Synonyms:2-Pyridineundecanol,4-hydroxy-5-methoxy-a,6-dimethyl-, (S)-; (+)-Melochinine; Melochinin; Melochinine, (+)-

Suppliers and Price of 6-[(11R)-11-hydroxydodecyl]-3-methoxy-2-methyl-1H-pyridin-4-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 3 raw suppliers

Chemical Property of 6-[(11R)-11-hydroxydodecyl]-3-methoxy-2-methyl-1H-pyridin-4-one

Chemical Property:

Vapor Pressure:1.53E-10mmHg at 25°C
Melting Point:145.5 - 147 °C
Boiling Point:463.5°Cat760mmHg
Flash Point:234.1°C
PSA：62.32000
Density:1.01g/cm³
LogP:4.12610

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 6-[(11R)-11-hydroxydodecyl]-3-methoxy-2-methyl-1H-pyridin-4-one

There total 3 articles about 6-[(11R)-11-hydroxydodecyl]-3-methoxy-2-methyl-1H-pyridin-4-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 83542-34-1
(+)-(S)-6-(11-Hydroxydodecyl)-3-methoxy-2-methyl-4-pyron

: 83542-30-7,70001-21-7
(+)-(S)-Melochinin

Guidance literature:: With ammonium hydroxide; In methanol; at 100 ℃; for 48h;
DOI:10.1002/jlac.198219820806

Reference yield:

: 83515-81-5,83542-32-9,83542-33-0
(+)-(S)-6-(11-Hydroxy-1-dodecen-1-yl)-3-methoxy-2-methyl-4-pyron

: 83542-30-7,70001-21-7
(+)-(S)-Melochinin

Guidance literature:: Multi-step reaction with 2 steps

1: H₂ / 10 percent Pd/C / methanol / 0.33 h

2: 6 M NH₃ / methanol / 48 h / 100 °C

With ammonium hydroxide; hydrogen; palladium on activated charcoal; In methanol;
DOI:10.1002/jlac.198219820806

Reference yield:

: 83515-79-1,83515-80-4
(+)-(S)-6-(2,11-Dihydroxydodecyl)-3-methoxy-2-methyl-4-pyron

: 83542-30-7,70001-21-7
(+)-(S)-Melochinin

Guidance literature:: Multi-step reaction with 3 steps

1: p-toluenesulfonic acid-hydrate / toluene / 0.75 h / 150 - 155 °C

2: H₂ / 10 percent Pd/C / methanol / 0.33 h

3: 6 M NH₃ / methanol / 48 h / 100 °C

With ammonium hydroxide; hydrogen; toluene-4-sulfonic acid; palladium on activated charcoal; In methanol; toluene;
DOI:10.1002/jlac.198219820806