Tricyclo(4.4.2.0(1,6))dodeca-2,4,7,9-tetraene

Base Information

• Chemical Name: Tricyclo(4.4.2.0(1,6))dodeca-2,4,7,9-tetraene
• CAS No.: 5181-34-0
• Molecular Formula: C₁₂H₁₂
• Molecular Weight: 156.227
• DSSTox Substance ID: DTXSID60199762
• Wikidata: Q83072726
• Mol file: 5181-34-0.mol

Synonyms:5181-34-0;Tricyclo(4.4.2.0(1,6))dodeca-2,4,7,9-tetraene;Tricyclo[4.4.2.0(1,6)dodeca-2,4,7,9-tetraene;DTXSID60199762

Chemical Property of Tricyclo(4.4.2.0(1,6))dodeca-2,4,7,9-tetraene

Chemical Property:

• Vapor Pressure: 0.00661mmHg at 25°C
• Refractive Index: 1.625
• Boiling Point: 280 °C at 760 mmHg
• Flash Point: 96.1 °C
• Density: 1.08 g/cm³
• XLogP3: 4
• Hydrogen Bond Donor Count: 0
• Hydrogen Bond Acceptor Count: 0
• Rotatable Bond Count: 0
• Exact Mass: 156.093900383
• Heavy Atom Count: 12
• Complexity: 268

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

• Canonical SMILES: C1CC23C1(C=CC=C2)C=CC=C3

Technology Process of Tricyclo(4.4.2.0(1,6))dodeca-2,4,7,9-tetraene

There total 2 articles about Tricyclo(4.4.2.0(1,6))dodeca-2,4,7,9-tetraene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

<4.4.2>-propella-3,8-diene (5103-78-6) → 9,10-Dihydro-9,10-aethano-naphthalin (5181-34-0)

Guidance literature:

Multistep reaction; (i) NBS, CCl₄, (ii) LiF, Li₂CO₃, HMPT;

DOI:10.1055/s-1977-24359

Reference yield:

→ 9,10-Dihydro-9,10-aethano-naphthalin (5181-34-0)

Guidance literature:

entspr. Hexahydro-Deriv. (VIII);

upstream raw materials:

<4.4.2>-propella-3,8-diene