Phosphoramidothioic acid, phenyl-, O,O-diethyl ester

Base Information

Chemical Name:Phosphoramidothioic acid, phenyl-, O,O-diethyl ester
CAS No.:3694-54-0
Molecular Formula:C10H16NO2PS
Molecular Weight:245.282
Hs Code.:
DSSTox Substance ID:DTXSID20190437
Wikidata:Q83062795
Mol file:3694-54-0.mol

Synonyms:Diethyl anilidothiophosphate;Phenylphosphoramidothioic acid O,O-diethyl ester;3694-54-0;BRN 2807729;Phosphoramidothioic acid, phenyl-, O,O-diethyl ester;4-12-00-01090 (Beilstein Handbook Reference);C10H16NO2PS;DTXSID20190437;C10-H16-N-O2-P-S;LS-107442

Suppliers and Price of Phosphoramidothioic acid, phenyl-, O,O-diethyl ester

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of Phosphoramidothioic acid, phenyl-, O,O-diethyl ester

Chemical Property:

Vapor Pressure:0.00105mmHg at 25°C
Boiling Point:301.5°Cat760mmHg
Flash Point:136.2°C
Density:1.207g/cm³
XLogP3:3.8
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:6
Exact Mass:245.06393692
Heavy Atom Count:15
Complexity:210

Purity/Quality:: 95% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCOP(=S)(NC1=CC=CC=C1)OCC

Technology Process of Phosphoramidothioic acid, phenyl-, O,O-diethyl ester

There total 5 articles about Phosphoramidothioic acid, phenyl-, O,O-diethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 38.0%

: 2524-04-1
diethyl phosphorochloridothioate

: 62-53-3
aniline

: 3694-54-0
O,O-diethyl N-phenylphosphoramidothioate

Guidance literature:: In toluene; for 72h; Heating;

Reference yield: 32.0%

: 5156-98-9
diethyl phenylphosphoramidite

: 3694-54-0
O,O-diethyl N-phenylphosphoramidothioate

: 86138-54-7
diethyl N-(diethoxyphosphinothioyl)-N,N'-diphenylphosphoramidimidate

Guidance literature:: With sulfur dichloride; triethylamine; In diethyl ether; Ambient temperature;

Reference yield:

: 62-53-3
aniline

: 3694-54-0
O,O-diethyl N-phenylphosphoramidothioate

Guidance literature:: Multi-step reaction with 2 steps

1: 28.1 percent / PSCl₃, NaOH / benzene; H₂O / 3 h / 0 °C

2: 15 percent Spectr_. / benzene; dioxane / 5 h / Ambient temperature

With sodium hydroxide; trichlorophosphate; In 1,4-dioxane; water; benzene;
DOI:10.1021/jo952270j