Silane, [[2-[2-[7-[(4-methylphenyl)sulfinyl]-2,6-dioxabicyclo[2.2.2]oct-1-yl]ethyl]-1 ,3-propanediyl]bis(oxy)]bis[(1,1-dimethylethyl)diphenyl-

Base Information

Chemical Name:Silane, [[2-[2-[7-[(4-methylphenyl)sulfinyl]-2,6-dioxabicyclo[2.2.2]oct-1-yl]ethyl]-1 ,3-propanediyl]bis(oxy)]bis[(1,1-dimethylethyl)diphenyl-
CAS No.:113477-00-2
Molecular Formula:C₅₀H₆₂O₅SSi₂
Molecular Weight:831.276
Hs Code.:
Mol file:113477-00-2.mol

Silane,
[[2-[2-[7-[(4-methylphenyl)sulfinyl]-2,6-dioxabicyclo[2.2.2]oct-1-yl]ethyl]-1
,3-propanediyl]bis(oxy)]bis[(1,1-dimethylethyl)diphenyl-

Synonyms:

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Chemical Property of Silane, [[2-[2-[7-[(4-methylphenyl)sulfinyl]-2,6-dioxabicyclo[2.2.2]oct-1-yl]ethyl]-1 ,3-propanediyl]bis(oxy)]bis[(1,1-dimethylethyl)diphenyl-

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Technology Process of Silane, [[2-[2-[7-[(4-methylphenyl)sulfinyl]-2,6-dioxabicyclo[2.2.2]oct-1-yl]ethyl]-1 ,3-propanediyl]bis(oxy)]bis[(1,1-dimethylethyl)diphenyl-

There total 6 articles about Silane, [[2-[2-[7-[(4-methylphenyl)sulfinyl]-2,6-dioxabicyclo[2.2.2]oct-1-yl]ethyl]-1 ,3-propanediyl]bis(oxy)]bis[(1,1-dimethylethyl)diphenyl- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 91.0%

: 113476-99-6
(R_S)-1,1-bis(tert-butyldiphenylsilyloxymethyl)-7,7-bis(hydroxymethyl)-5-(p-tolyl)sulfinyl-4-heptanone

: 113477-00-2
1-[4-(tert-Butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-butyl]-7-((S)-toluene-4-sulfinyl)-2,6-dioxa-bicyclo[2.2.2]octane

Guidance literature:: With zinc(II) chloride;
DOI:10.1016/S0040-4039(00)96304-4

Reference yield:

: 1519-39-7
(R)-methyl p-tolyl sulfoxide

: 113477-00-2
1-[4-(tert-Butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-butyl]-7-((S)-toluene-4-sulfinyl)-2,6-dioxa-bicyclo[2.2.2]octane

Guidance literature:: Multi-step reaction with 4 steps

1: 84 percent

2: 87 percent

4: 91 percent / ZnCl₂

With zinc(II) chloride;
DOI:10.1016/S0040-4039(00)96304-4

Reference yield:

: 113457-95-7
4,4-bis(hydroxymethyl)butanal ethylene acetal

: 113477-00-2
1-[4-(tert-Butyl-diphenyl-silanyloxy)-3-(tert-butyl-diphenyl-silanyloxymethyl)-butyl]-7-((S)-toluene-4-sulfinyl)-2,6-dioxa-bicyclo[2.2.2]octane

Guidance literature:: Multi-step reaction with 5 steps

1: 1.)imidazole; 2.) p-TsOH / 2.) acetone

2: 84 percent

3: 87 percent

5: 91 percent / ZnCl₂

With 1H-imidazole; toluene-4-sulfonic acid; zinc(II) chloride;
DOI:10.1016/S0040-4039(00)96304-4