Technology Process of 1,3-Dioxolane-2-propanol, a-3,7-dodecadienyl-,
4-methylbenzenesulfonate, (Z,Z)-
There total 19 articles about 1,3-Dioxolane-2-propanol, a-3,7-dodecadienyl-,
4-methylbenzenesulfonate, (Z,Z)- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 100 percent / pyridine / 20 h / 0 °C
2: 95 percent / 10percent aq. HCl / acetone / 6 h
3: 1.) Mg / 1.) THF, 2.) THF, RT, 3 h
4: pyridine / 20 h / 0 °C
With
pyridine; hydrogenchloride; magnesium;
In
acetone;
- Guidance literature:
-
Multi-step reaction with 6 steps
1: p-toluenesulfonic acid / 24 h / Ambient temperature
2: 90 percent / diisobutylaluminium hydride / diethyl ether; toluene / 1.5 h / -10 °C
3: 100 percent / pyridine / 20 h / 0 °C
4: 95 percent / 10percent aq. HCl / acetone / 6 h
5: 1.) Mg / 1.) THF, 2.) THF, RT, 3 h
6: pyridine / 20 h / 0 °C
With
pyridine; hydrogenchloride; diisobutylaluminium hydride; toluene-4-sulfonic acid; magnesium;
In
diethyl ether; acetone; toluene;
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 90 percent / diisobutylaluminium hydride / diethyl ether; toluene / 1.5 h / -10 °C
2: 100 percent / pyridine / 20 h / 0 °C
3: 95 percent / 10percent aq. HCl / acetone / 6 h
4: 1.) Mg / 1.) THF, 2.) THF, RT, 3 h
5: pyridine / 20 h / 0 °C
With
pyridine; hydrogenchloride; diisobutylaluminium hydride; magnesium;
In
diethyl ether; acetone; toluene;
