3-(4-methylphenyl)-6-phenyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Base Information

Chemical Name:3-(4-methylphenyl)-6-phenyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole
CAS No.:113486-83-2
Molecular Formula:C₁₆H₁₂N₄S
Molecular Weight:292.364
Hs Code.:
Mol file:113486-83-2.mol

Synonyms:6-Phenyl-3-p-tolyl-[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole;

Suppliers and Price of 3-(4-methylphenyl)-6-phenyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3-(4-methylphenyl)-6-phenyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

Chemical Property:

PSA：71.32000
LogP:3.82820

Purity/Quality:

Safty Information:

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Technology Process of 3-(4-methylphenyl)-6-phenyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole

There total 3 articles about 3-(4-methylphenyl)-6-phenyl[1,2,4]triazolo[3,4-b][1,3,4]thiadiazole which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 86.0%

: 13229-01-1
4-amino-2,4-dihydro-5-(4-methylphenyl)-3H-1,2,4-triazole-3-thione

: 65-85-0,8013-63-6
benzoic acid

: 113486-83-2
6-Phenyl-3-(4-tolyl)-s-triazolo<3,4-b><1,3,4>thiadiazole

Guidance literature:: With trichlorophosphate; for 1h; Heating;

Reference yield:

: 38499-94-4
potassium 3-p-toluoyldithiocarbazate

: 113486-83-2
6-Phenyl-3-(4-tolyl)-s-triazolo<3,4-b><1,3,4>thiadiazole

Guidance literature:: Multi-step reaction with 2 steps

1: 56 percent / H₂NNH₂*H₂O / H₂O / 12 h / Heating

2: 50 percent / POCl₃ / 5 h / Heating

With hydrazine hydrate; trichlorophosphate; In water;

Reference yield:

: 3619-22-5
p-toluic hydrazide

: 113486-83-2
6-Phenyl-3-(4-tolyl)-s-triazolo<3,4-b><1,3,4>thiadiazole

Guidance literature:: Multi-step reaction with 3 steps

1: KOH / ethanol / 16 h / Ambient temperature

2: 56 percent / H₂NNH₂*H₂O / H₂O / 12 h / Heating

3: 50 percent / POCl₃ / 5 h / Heating

With potassium hydroxide; hydrazine hydrate; trichlorophosphate; In ethanol; water;