Technology Process of Benzoic acid,
3-(2-carboxy-5-methoxy-3-propylphenoxy)-4,6-dihydroxy-2-pentyl-
There total 6 articles about Benzoic acid,
3-(2-carboxy-5-methoxy-3-propylphenoxy)-4,6-dihydroxy-2-pentyl- which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
With
hydrogen;
palladium on activated charcoal;
In
ethyl acetate;
for 15h;
DOI:10.1071/CH9871451
- Guidance literature:
-
Multi-step reaction with 6 steps
1: 43 percent / potassium carbonate / acetone / 22 h / Heating
2: 19 percent / potassium persulfate, 20percent sodium hydroxide, dimethyl sulfoxide / 24 h / 10 - 20 °C
3: 76 percent / trifluofoacetic anhydride / toluene / 2 h / Ambient temperature
4: 13 percent / potassium carbonate / dimethylsulfoxide / 75 - 76 °C
5: 36 percent / potassium hydroxide / dimethylsulfoxide / 8 h / 90 - 95 °C
6: 98 percent / H2 / 10percent Pd/C / ethyl acetate / 15 h
With
potassium hydroxide; sodium hydroxide; potassium peroxomonosulphate; hydrogen; potassium carbonate; dimethyl sulfoxide; trifluoroacetic anhydride;
palladium on activated charcoal;
In
dimethyl sulfoxide; ethyl acetate; acetone; toluene;
DOI:10.1071/CH9871451
- Guidance literature:
-
Multi-step reaction with 5 steps
1: 19 percent / potassium persulfate, 20percent sodium hydroxide, dimethyl sulfoxide / 24 h / 10 - 20 °C
2: 76 percent / trifluofoacetic anhydride / toluene / 2 h / Ambient temperature
3: 13 percent / potassium carbonate / dimethylsulfoxide / 75 - 76 °C
4: 36 percent / potassium hydroxide / dimethylsulfoxide / 8 h / 90 - 95 °C
5: 98 percent / H2 / 10percent Pd/C / ethyl acetate / 15 h
With
potassium hydroxide; sodium hydroxide; potassium peroxomonosulphate; hydrogen; potassium carbonate; dimethyl sulfoxide; trifluoroacetic anhydride;
palladium on activated charcoal;
In
dimethyl sulfoxide; ethyl acetate; toluene;
DOI:10.1071/CH9871451
