Cyclohexanecarboxylic acid, 4-acetyl-2-(2-propynyl)-, 1,1-dimethylethyl ester

Base Information

Chemical Name:Cyclohexanecarboxylic acid, 4-acetyl-2-(2-propynyl)-, 1,1-dimethylethyl ester
CAS No.:113507-69-0
Molecular Formula:C₁₆H₂₄O₃
Molecular Weight:264.365
Hs Code.:
Mol file:113507-69-0.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Cyclohexanecarboxylic acid, 4-acetyl-2-(2-propynyl)-, 1,1-dimethylethyl ester

Chemical Property:

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Technology Process of Cyclohexanecarboxylic acid, 4-acetyl-2-(2-propynyl)-, 1,1-dimethylethyl ester

There total 13 articles about Cyclohexanecarboxylic acid, 4-acetyl-2-(2-propynyl)-, 1,1-dimethylethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 4893-15-6
1-(4-methoxy-cyclohex-3-enyl)-ethanone

: 113507-69-0
4-Acetyl-2-prop-2-ynyl-cyclohexanecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 13 steps

1: NaBH₄

2: hydrolysis

4: NaH

6: 81 percent / LDA

7: 90 percent

8: 1.) CF₃CO₂H; 2.) H₂O₂, NaOH / 1.) CH₃CN, H₂O

9: K₂CO₃

10: BF₃, EtSH

11: CrO₃, acid

12: hydrolysis

13: thionyl chloride

With chromium(VI) oxide; sodium hydroxide; sodium tetrahydroborate; thionyl chloride; boron trifluoride; dihydrogen peroxide; sodium hydride; potassium carbonate; trifluoroacetic acid; ethanethiol; lithium diisopropyl amide;
DOI:10.1021/ja00215a058

Reference yield:

: 113507-58-7
1-(4-Methoxy-cyclohex-3-enyl)-ethanol

: 113507-69-0
4-Acetyl-2-prop-2-ynyl-cyclohexanecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 12 steps

1: hydrolysis

3: NaH

5: 81 percent / LDA

6: 90 percent

7: 1.) CF₃CO₂H; 2.) H₂O₂, NaOH / 1.) CH₃CN, H₂O

8: K₂CO₃

9: BF₃, EtSH

10: CrO₃, acid

11: hydrolysis

12: thionyl chloride

With chromium(VI) oxide; sodium hydroxide; thionyl chloride; boron trifluoride; dihydrogen peroxide; sodium hydride; potassium carbonate; trifluoroacetic acid; ethanethiol; lithium diisopropyl amide;
DOI:10.1021/ja00215a058

Reference yield:

: 113507-59-8
4-(hydroxyethyl)cyclohexanone

: 113507-69-0
4-Acetyl-2-prop-2-ynyl-cyclohexanecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 11 steps

2: NaH

4: 81 percent / LDA

5: 90 percent

6: 1.) CF₃CO₂H; 2.) H₂O₂, NaOH / 1.) CH₃CN, H₂O

7: K₂CO₃

8: BF₃, EtSH

9: CrO₃, acid

10: hydrolysis

11: thionyl chloride

With chromium(VI) oxide; sodium hydroxide; thionyl chloride; boron trifluoride; dihydrogen peroxide; sodium hydride; potassium carbonate; trifluoroacetic acid; ethanethiol; lithium diisopropyl amide;
DOI:10.1021/ja00215a058