1,2,4-Benzenetriol, 3,5-dichloro-6-(1-propenyl)-, triacetate, (E)-

Base Information

Chemical Name:1,2,4-Benzenetriol, 3,5-dichloro-6-(1-propenyl)-, triacetate, (E)-
CAS No.:113524-16-6
Molecular Formula:C₁₅H₁₄Cl₂O₆
Molecular Weight:361.179
Hs Code.:
Mol file:113524-16-6.mol

Synonyms:

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Chemical Property of 1,2,4-Benzenetriol, 3,5-dichloro-6-(1-propenyl)-, triacetate, (E)-

Chemical Property:

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Technology Process of 1,2,4-Benzenetriol, 3,5-dichloro-6-(1-propenyl)-, triacetate, (E)-

There total 17 articles about 1,2,4-Benzenetriol, 3,5-dichloro-6-(1-propenyl)-, triacetate, (E)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 27971-69-3
2‐chloro‐1,3‐dimethoxy‐5‐methyl benzene

: 113524-16-6
(E)-1-(2,3,5-triacetoxy-4,6-dichlorophenyl)prop-1-ene

Guidance literature:: Multi-step reaction with 15 steps

1: 62 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h / 0 °C

2: 85 percent / K₂CO₃ / butan-2-one / 5 h / Heating

3: 97 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating; Irradiation

4: 98 percent / aq. AgNO₃ / 2-methoxy-ethanol / 0.5 h / Heating

5: 84 percent / tetrabutylammonium permanganate / pyridine / 16 h / 4 °C

6: 84 percent / AlCl₃ / chlorobenzene / 0.75 h / Heating

7: 79 percent / HCl / 4 h / Heating

8: 86 percent / K₂CO₃ / butan-2-one / 16 h / Heating

9: 84 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h

10: 91 percent / NaBH₄ / methanol / 1 h / 0 °C

11: 97 percent / pyridine / 16 h

12: 88 percent / SO₂Cl₂ / diethyl ether / 3 h / Ambient temperature

13: 83 percent / 5 M aq. NaOH / ethanol / 2 h / Heating

14: H₂ / 10percent Pd/C / methanol / 1 h / 760 Torr

15: 1.) trifluoroacetic acid; 2.) pyridine / methanol / Ambient temperature; 1.) 16 h; 2.) 5 h

With pyridine; hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; aluminium trichloride; sulfuryl dichloride; tetra-n-butylammonium permanganate; hexane; hydrogen; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; diethyl ether; ethanol; dichloromethane; 2-methoxy-ethanol; chlorobenzene; butanone;

Reference yield:

: 56021-31-9
4-chloro-3,5-dihydroxytoluene

: 113524-16-6
(E)-1-(2,3,5-triacetoxy-4,6-dichlorophenyl)prop-1-ene

Guidance literature:: Multi-step reaction with 16 steps

1: 86 percent / K₂CO₃ / butan-2-one / 5 h / Heating

2: 62 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h / 0 °C

3: 85 percent / K₂CO₃ / butan-2-one / 5 h / Heating

4: 97 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating; Irradiation

5: 98 percent / aq. AgNO₃ / 2-methoxy-ethanol / 0.5 h / Heating

6: 84 percent / tetrabutylammonium permanganate / pyridine / 16 h / 4 °C

7: 84 percent / AlCl₃ / chlorobenzene / 0.75 h / Heating

8: 79 percent / HCl / 4 h / Heating

9: 86 percent / K₂CO₃ / butan-2-one / 16 h / Heating

10: 84 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h

11: 91 percent / NaBH₄ / methanol / 1 h / 0 °C

12: 97 percent / pyridine / 16 h

13: 88 percent / SO₂Cl₂ / diethyl ether / 3 h / Ambient temperature

14: 83 percent / 5 M aq. NaOH / ethanol / 2 h / Heating

15: H₂ / 10percent Pd/C / methanol / 1 h / 760 Torr

16: 1.) trifluoroacetic acid; 2.) pyridine / methanol / Ambient temperature; 1.) 16 h; 2.) 5 h

With pyridine; hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; aluminium trichloride; sulfuryl dichloride; tetra-n-butylammonium permanganate; hexane; hydrogen; potassium carbonate; silver nitrate; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; diethyl ether; ethanol; dichloromethane; 2-methoxy-ethanol; chlorobenzene; butanone;

Reference yield:

: 4179-19-5
1,3-dimethoxy-5-methylbenzene

: 113524-16-6
(E)-1-(2,3,5-triacetoxy-4,6-dichlorophenyl)prop-1-ene

Guidance literature:: Multi-step reaction with 16 steps

1: 62 percent / 1.) BuLi; 2.) 1,2-dichloroethane / 1.) ether, r.t., 72 h; 2.) ether, reflux, 1.5 h

2: 62 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 5 h / 0 °C

3: 85 percent / K₂CO₃ / butan-2-one / 5 h / Heating

4: 97 percent / N-bromosuccinimide / CCl₄ / 1.5 h / Heating; Irradiation

5: 98 percent / aq. AgNO₃ / 2-methoxy-ethanol / 0.5 h / Heating

6: 84 percent / tetrabutylammonium permanganate / pyridine / 16 h / 4 °C

7: 84 percent / AlCl₃ / chlorobenzene / 0.75 h / Heating

8: 79 percent / HCl / 4 h / Heating

9: 86 percent / K₂CO₃ / butan-2-one / 16 h / Heating

10: 84 percent / 1.) buthyl-lithium/hexane / tetrahydrofuran / 1.) -50 deg C, 3 h; 2.) -78 deg C, 2 h

11: 91 percent / NaBH₄ / methanol / 1 h / 0 °C

12: 97 percent / pyridine / 16 h

13: 88 percent / SO₂Cl₂ / diethyl ether / 3 h / Ambient temperature

14: 83 percent / 5 M aq. NaOH / ethanol / 2 h / Heating

15: H₂ / 10percent Pd/C / methanol / 1 h / 760 Torr

16: 1.) trifluoroacetic acid; 2.) pyridine / methanol / Ambient temperature; 1.) 16 h; 2.) 5 h

With pyridine; hydrogenchloride; sodium hydroxide; sodium tetrahydroborate; N-Bromosuccinimide; n-butyllithium; aluminium trichloride; sulfuryl dichloride; tetra-n-butylammonium permanganate; hexane; hydrogen; potassium carbonate; silver nitrate; 1,2-dichloro-ethane; 3-chloro-benzenecarboperoxoic acid; trifluoroacetic acid; palladium on activated charcoal; In tetrahydrofuran; pyridine; methanol; tetrachloromethane; diethyl ether; ethanol; dichloromethane; 2-methoxy-ethanol; chlorobenzene; butanone;