2-(2-(Methylamino)ethyl)phthalazin-1(2H)-one

Base Information

Chemical Name:2-(2-(Methylamino)ethyl)phthalazin-1(2H)-one
CAS No.:113582-15-3
Molecular Formula:C11H13N3O
Molecular Weight:203.24000
Hs Code.:
DSSTox Substance ID:DTXSID10601128
Wikidata:Q82497585
Mol file:113582-15-3.mol

Synonyms:113582-15-3;2-(2-(METHYLAMINO)ETHYL)PHTHALAZIN-1(2H)-ONE;2-[2-(methylamino)ethyl]phthalazin-1-one;2-[2-(methylamino)ethyl]-1-phthalazinone;2-(2-methylamino-ethyl)-2H-phthalazin-1-one;2-[2-(methylamino)ethyl]-1,2-dihydrophthalazin-1-one;2-[2-(Methylamino)ethyl]phthalazin-1(2H)-one;SCHEMBL3973342;DTXSID10601128;WAPQGASETVZFBS-UHFFFAOYSA-N;AKOS010645922;DB-002387;N-methyl-2-(phthalazin-1-on-2-yl)ethylamine;F52445;EN300-9145195;A803072;2-[2-(Methylamino)ethyl]-1(2H)-phthalazinone, AldrichCPR

Suppliers and Price of 2-(2-(Methylamino)ethyl)phthalazin-1(2H)-one

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 2 raw suppliers

Chemical Property of 2-(2-(Methylamino)ethyl)phthalazin-1(2H)-one

Chemical Property:

PSA：46.92000
LogP:1.00680
XLogP3:0.2
Hydrogen Bond Donor Count:1
Hydrogen Bond Acceptor Count:3
Rotatable Bond Count:3
Exact Mass:203.105862047
Heavy Atom Count:15
Complexity:265

Purity/Quality:: 97% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CNCCN1C(=O)C2=CC=CC=C2C=N1

Technology Process of 2-(2-(Methylamino)ethyl)phthalazin-1(2H)-one

There total 3 articles about 2-(2-(Methylamino)ethyl)phthalazin-1(2H)-one which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 81.0%

: 1146480-72-9
N,4-dimethyl-N-[2-((1-oxo-1H-phthalazin-2)-yl)ethyl]benzenesulfonamide

: 113582-15-3
2-[2-(methylamino)-ethyl]-2H-phthalazin-1-one

Guidance literature:: N,4-dimethyl-N-[2-((1-oxo-1H-phthalazin-2)-yl)ethyl]benzenesulfonamide; With sulfuric acid; at 100 - 110 ℃; for 6h;

With sodium hydroxide; In water; at 20 ℃;

Reference yield:

: methyl-[2-(1-oxo-1H-phthalazin-2-yl)ethyl]carbamic acid tert-butyl ester

: 113582-15-3
2-[2-(methylamino)-ethyl]-2H-phthalazin-1-one

Guidance literature:: With hydrogenchloride; In water; at 20 ℃; for 30h;
DOI:10.1080/00397911.2014.944269

Reference yield:

: 119-39-1
phthalazone

: 113582-15-3
2-[2-(methylamino)-ethyl]-2H-phthalazin-1-one

Guidance literature:: Multi-step reaction with 2 steps

1.1: sodium methylate / methanol / 0.5 h / Heating

1.2: 7 h / Heating

2.1: sulfuric acid / 6 h / 100 - 110 °C

With sulfuric acid; sodium methylate; In methanol;
DOI:10.1080/00397911.2014.944269