1H-Pyrrole-2-carboxamide, N-(3-amino-3-iminopropyl)-4-[[(4-amino-1H-pyrrol-2-yl)carbonyl]amino]- 1-methyl-, monohydrochloride

Base Information

Chemical Name:1H-Pyrrole-2-carboxamide, N-(3-amino-3-iminopropyl)-4-[[(4-amino-1H-pyrrol-2-yl)carbonyl]amino]- 1-methyl-, monohydrochloride
CAS No.:113598-32-6
Molecular Formula:C14H19N7O2.ClH
Molecular Weight:353.812
Hs Code.:
Mol file:113598-32-6.mol

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Chemical Property of 1H-Pyrrole-2-carboxamide, N-(3-amino-3-iminopropyl)-4-[[(4-amino-1H-pyrrol-2-yl)carbonyl]amino]- 1-methyl-, monohydrochloride

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Technology Process of 1H-Pyrrole-2-carboxamide, N-(3-amino-3-iminopropyl)-4-[[(4-amino-1H-pyrrol-2-yl)carbonyl]amino]- 1-methyl-, monohydrochloride

There total 1 articles about 1H-Pyrrole-2-carboxamide, N-(3-amino-3-iminopropyl)-4-[[(4-amino-1H-pyrrol-2-yl)carbonyl]amino]- 1-methyl-, monohydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 5930-93-8
4-nitropyrrole-2-carboxylic acid

: 113598-32-6
4-[(4-Amino-1H-pyrrole-2-carbonyl)-amino]-1-methyl-1H-pyrrole-2-carboxylic acid (2-carbamimidoyl-ethyl)-amide; hydrochloride

Guidance literature:: Multi-step reaction with 4 steps

1: Et₃N, SOCl₂ / 1,2-dimethoxy-ethane / 0.25 h / 0 °C

2: 70 percent / Et₃N / tetrahydrofuran; CH₂Cl₂ / 1.) -20 deg C, 15 min, 2.) RT, 16 h

3: 1.) HCl gas, 2.) NH₃ gas / 1.) EtOH, a) 0 deg C, 1 h, b) RT, 30 min, 2.) EtOH, 0 deg C, 50 min

4: H₂ / 10percent Pd/C / methanol / 760 Torr / Ambient temperature

With hydrogenchloride; thionyl chloride; ammonia; hydrogen; triethylamine; palladium on activated charcoal; In tetrahydrofuran; methanol; 1,2-dimethoxyethane; dichloromethane;
DOI:10.1021/jo00244a003