3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,4,6-trimethyl-, 2-[(2-hydroxybenzoyl)amino]ethyl 2-(3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester, S,S-dioxide

Base Information

Chemical Name:3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,4,6-trimethyl-, 2-[(2-hydroxybenzoyl)amino]ethyl 2-(3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester, S,S-dioxide
CAS No.:113658-87-0
Molecular Formula:C₂₈H₂₉N₃O₉S
Molecular Weight:583.619
Hs Code.:
Mol file:113658-87-0.mol

3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,4,6-trimethyl-,
2-[(2-hydroxybenzoyl)amino]ethyl
2-(3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester, S,S-dioxide

Synonyms:

Suppliers and Price of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,4,6-trimethyl-, 2-[(2-hydroxybenzoyl)amino]ethyl 2-(3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester, S,S-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,4,6-trimethyl-, 2-[(2-hydroxybenzoyl)amino]ethyl 2-(3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester, S,S-dioxide

Chemical Property:

Purity/Quality:: 99.90% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,4,6-trimethyl-, 2-[(2-hydroxybenzoyl)amino]ethyl 2-(3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester, S,S-dioxide

There total 4 articles about 3,5-Pyridinedicarboxylic acid, 1,4-dihydro-2,4,6-trimethyl-, 2-[(2-hydroxybenzoyl)amino]ethyl 2-(3-oxo-1,2-benzisothiazol-2(3H)-yl)ethyl ester, S,S-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

: 75-07-0,9002-91-9
acetaldehyde

: 113658-92-7
2-(1,1,3-trioxo-2,3-dihydro-1,2-benzisothiazol-2-yl)ethyl acetylacetate

: 92565-10-1
2-(2-salicylamido)ethyl 3-aminocrotonate

: 113658-87-0
2,4,6-Trimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-[2-(2-hydroxy-benzoylamino)-ethyl] ester 5-[2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl] ester

Guidance literature:: In ethanol; for 10h; Heating;
DOI:10.1021/jm00118a004

Reference yield:

: 24207-38-3
N-(2-hydroxyethyl)salicylamide

: 113658-87-0
2,4,6-Trimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-[2-(2-hydroxy-benzoylamino)-ethyl] ester 5-[2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 3 steps

1: 76 percent / Et₃N / ethane-1,2-diamine / 3 h

2: 80 percent / NH₃ / methanol / 3 h

3: 46 percent / ethanol / 10 h / Heating

With ammonia; triethylamine; In methanol; ethanol; ethylenediamine;
DOI:10.1021/jm00118a004

Reference yield:

: 6343-81-3
2-(2-hydroxyethyl)-1,2-benzisothiazol-3(2H)-one 1,1-dioxide

: 113658-87-0
2,4,6-Trimethyl-1,4-dihydro-pyridine-3,5-dicarboxylic acid 3-[2-(2-hydroxy-benzoylamino)-ethyl] ester 5-[2-(1,1,3-trioxo-1,3-dihydro-1λ⁶-benzo[d]isothiazol-2-yl)-ethyl] ester

Guidance literature:: Multi-step reaction with 2 steps

1: 88 percent / Et₃N / 3 h / 90 °C

2: 46 percent / ethanol / 10 h / Heating

With triethylamine; In ethanol;
DOI:10.1021/jm00118a004