Technology Process of Benzoic acid, 4-(decyloxy)-, 4-[(2-fluorooctyl)oxy]phenyl ester, (S)-
There total 4 articles about Benzoic acid, 4-(decyloxy)-, 4-[(2-fluorooctyl)oxy]phenyl ester, (S)- which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
Multi-step reaction with 3 steps
1: 71 percent / pyridine / 6 h / Ambient temperature
2: 54 percent / NaOH / butan-1-ol / 6 h / 120 °C
3: 1) triethylenediamine, 2) sodium hydride / 1) benzene, 60 deg C, 2 h, 2) 90 deg C, 3 h
With
1,4-diaza-bicyclo[2.2.2]octane; sodium hydroxide; sodium hydride;
In
pyridine; butan-1-ol;
- Guidance literature:
-
Multi-step reaction with 2 steps
1: 54 percent / NaOH / butan-1-ol / 6 h / 120 °C
2: 1) triethylenediamine, 2) sodium hydride / 1) benzene, 60 deg C, 2 h, 2) 90 deg C, 3 h
With
1,4-diaza-bicyclo[2.2.2]octane; sodium hydroxide; sodium hydride;
In
butan-1-ol;
- Guidance literature:
-
Multi-step reaction with 4 steps
1: 41 percent / pyridinium poly(hydrogen fluoride) / diethyl ether / 3 h
2: 71 percent / pyridine / 6 h / Ambient temperature
3: 54 percent / NaOH / butan-1-ol / 6 h / 120 °C
4: 1) triethylenediamine, 2) sodium hydride / 1) benzene, 60 deg C, 2 h, 2) 90 deg C, 3 h
With
1,4-diaza-bicyclo[2.2.2]octane; sodium hydroxide; sodium hydride; pyridine hydrogenfluoride;
In
pyridine; diethyl ether; butan-1-ol;
