Carbamothioic acid, [(2-benzothiazolylthio)methyl](2,6-diethylphenyl)-, S-2-benzothiazolyl ester

Base Information

• Chemical Name: Carbamothioic acid, [(2-benzothiazolylthio)methyl](2,6-diethylphenyl)-, S-2-benzothiazolyl ester
• CAS No.: 113707-98-5
• Molecular Formula: C₂₆H₂₃N₃OS₄
• Molecular Weight: 521.752
• Mol file: 113707-98-5.mol

Synonyms:

Chemical Property of Carbamothioic acid, [(2-benzothiazolylthio)methyl](2,6-diethylphenyl)-, S-2-benzothiazolyl ester

Chemical Property:

Purity/Quality:

99.90% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Carbamothioic acid, [(2-benzothiazolylthio)methyl](2,6-diethylphenyl)-, S-2-benzothiazolyl ester

There total 2 articles about Carbamothioic acid, [(2-benzothiazolylthio)methyl](2,6-diethylphenyl)-, S-2-benzothiazolyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

2,6-diethyl-N-methylene-aniline (35203-08-8) → 2-benzothiazolyl-N-(2-benzothiazolylthiomethyl)-2,6-diethylthiolcarbanilate (113707-98-5)

Guidance literature:

Multi-step reaction with 2 steps

1: 74 percent / benzene / 1.) 25-30 deg C, 2 d; 2.) reflux, 2 h

2: 1.) 85percent KOH / 1.) acetone, reflux, 30 min; 2.) reflux, 5 h, then 25-30 deg C, 24 h

With potassium hydroxide; In benzene;

Reference yield:

N-(chloromethyl)-2,6-diethylcarbaniloyl chloride (35747-79-6) + 2-Mercaptobenzothiazole (149-30-4,118090-09-8) → 2-benzothiazolyl-N-(2-benzothiazolylthiomethyl)-2,6-diethylthiolcarbanilate (113707-98-5)

Guidance literature:

With potassium hydroxide; Yield given. Multistep reaction; 1.) acetone, reflux, 30 min; 2.) reflux, 5 h, then 25-30 deg C, 24 h;

upstream raw materials:

N-(chloromethyl)-2,6-diethylcarbaniloyl chloride

2-Mercaptobenzothiazole

2,6-diethyl-N-methylene-aniline

Refernces