Carbamothioic acid, (2,6-diethylphenyl)[[(4,6-dimethyl-2-pyrimidinyl)thio]methyl]-, S-(4,6-dimethyl-2-pyrimidinyl) ester

Base Information

Chemical Name:Carbamothioic acid, (2,6-diethylphenyl)[[(4,6-dimethyl-2-pyrimidinyl)thio]methyl]-, S-(4,6-dimethyl-2-pyrimidinyl) ester
CAS No.:113708-02-4
Molecular Formula:C₂₄H₂₉N₅OS₂
Molecular Weight:467.659
Hs Code.:
Mol file:113708-02-4.mol

Synonyms:

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Chemical Property of Carbamothioic acid, (2,6-diethylphenyl)[[(4,6-dimethyl-2-pyrimidinyl)thio]methyl]-, S-(4,6-dimethyl-2-pyrimidinyl) ester

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Technology Process of Carbamothioic acid, (2,6-diethylphenyl)[[(4,6-dimethyl-2-pyrimidinyl)thio]methyl]-, S-(4,6-dimethyl-2-pyrimidinyl) ester

There total 2 articles about Carbamothioic acid, (2,6-diethylphenyl)[[(4,6-dimethyl-2-pyrimidinyl)thio]methyl]-, S-(4,6-dimethyl-2-pyrimidinyl) ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 35203-08-8
2,6-diethyl-N-methylene-aniline

: 113708-02-4
4,6-dimethyl-2-pyrimidinyl-N-(2,6-diethylphenyl)-N-(4,6-dimethyl-2-pyrimidinylthiomethyl)thiolcarbanilate

Guidance literature:: Multi-step reaction with 2 steps

1: 74 percent / benzene / 1.) 25-30 deg C, 2 d; 2.) reflux, 2 h

2: 1.) 85percent KOH / 1.) acetone, reflux, 30 min; 2.) reflux, 5 h, then 25-30 deg C, 24 h

With potassium hydroxide; In benzene;

Reference yield:

: 35747-79-6
N-(chloromethyl)-2,6-diethylcarbaniloyl chloride

: 22325-27-5,131321-42-1
4,6-dimethyl-2-meraptopyrimidine

: 113708-02-4
4,6-dimethyl-2-pyrimidinyl-N-(2,6-diethylphenyl)-N-(4,6-dimethyl-2-pyrimidinylthiomethyl)thiolcarbanilate

Guidance literature:: With potassium hydroxide; Yield given. Multistep reaction; 1.) acetone, reflux, 30 min; 2.) reflux, 5 h, then 25-30 deg C, 24 h;