2-bromo-N-octylacetamide

Base Information

• Chemical Name: 2-bromo-N-octylacetamide
• CAS No.: 5326-97-6
• Molecular Formula: C10H20BrNO
• Molecular Weight: 250.1759
• Mol file: 5326-97-6.mol

Synonyms:

Chemical Property of 2-bromo-N-octylacetamide

Chemical Property:

• Vapor Pressure: 8.54E-05mmHg at 25°C
• Boiling Point: 340.5°Cat760mmHg
• Flash Point: 159.8°C
• Density: 1.176g/cm³

Purity/Quality:

99% ^*data from raw suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

Useful:

Technology Process of 2-bromo-N-octylacetamide

There total 5 articles about 2-bromo-N-octylacetamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 100.0%

n-Octylamine (111-86-4) + 2-Bromoacetyl bromide (598-21-0) → 2-Bromo-N-(n-octyl)acetamide (5326-97-6)

Guidance literature:

With potassium carbonate; In methanol; dichloromethane; at 25 ℃; for 1h;

DOI:10.1055/s-2002-19803

Reference yield: 91.0%

n-Octylamine (111-86-4) + bromoacetic acid (79-08-3) → 2-Bromo-N-(n-octyl)acetamide (5326-97-6)

Guidance literature:

With dicyclohexyl-carbodiimide; In dichloromethane; at 20 ℃; for 3h;

DOI:10.1016/S0223-5234(03)00059-X

Reference yield:

2-Bromoacetyl bromide (598-21-0) → 2-Bromo-N-(n-octyl)acetamide (5326-97-6)

Guidance literature:

With 1,2-dichloro-ethane; at -10 ℃;

upstream raw materials:

2-Bromoacetyl bromide

n-Octylamine

bromoacetic acid

octyl-carbamic acid tert-butyl ester

Refernces

• 1、 Gathergood, Nicholas,Ghosh, Kallol K.,Kapitanov, Illia V.,Karpichev, Yevgen,Pandya, Subhashree Jayesh,Sahu, Reshma,Sinha, Deepak,Usmani, Zeba. "An example of green surfactant systems based on inherently biodegradable IL-derived amphiphilic oximes". . . Retrieved 2020/03/18.
• 2、 Dey, Rajib,De, Kathakali,Mukherjee, Riya,Ghosh, Sreyan,Haldar, Jayanta. "Small antibacterial molecules highly active against drug-resistant: Staphylococcus aureus". supporting information. p. 1907 - 1915. Retrieved 2019/11/20.