1(2H)-Pyridinecarboxylic acid, 4,5-dimethyl-2-phenyl-, phenylmethyl ester

Base Information

Chemical Name:1(2H)-Pyridinecarboxylic acid, 4,5-dimethyl-2-phenyl-, phenylmethyl ester
CAS No.:113730-68-0
Molecular Formula:C21H21NO2
Molecular Weight:
Hs Code.:
Mol file:113730-68-0.mol

Synonyms:

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Chemical Property of 1(2H)-Pyridinecarboxylic acid, 4,5-dimethyl-2-phenyl-, phenylmethyl ester

Chemical Property:

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Technology Process of 1(2H)-Pyridinecarboxylic acid, 4,5-dimethyl-2-phenyl-, phenylmethyl ester

There total 1 articles about 1(2H)-Pyridinecarboxylic acid, 4,5-dimethyl-2-phenyl-, phenylmethyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 583-58-4
3,4-Lutidin

: phenylmagnesium bromide

: 501-53-1,94274-21-2
benzyl chloroformate

: 113730-68-0
1-benzyloxycarbonyl-4,5-dimethyl-2-phenyl-1,2-dihydropyridine

Guidance literature:: In tetrahydrofuran; at -5 ℃; for 2h;

Reference yield:

: 113730-68-0
1-benzyloxycarbonyl-4,5-dimethyl-2-phenyl-1,2-dihydropyridine

: 113730-72-6
2,4-Dimethyl-7-phenyl-3-oxa-6-aza-tricyclo[3.2.0.0^2,4]heptane

Guidance literature:: Multi-step reaction with 3 steps

1: CH₂Cl₂ / 22 h / Irradiation

2: 94 percent / m-chloroperbenzoic acid / CH₂Cl₂ / 48 h / Ambient temperature

3: 73 percent / H₂ / Pd-C (5percent) / ethyl acetate / 760 Torr / Ambient temperature

With hydrogen; 3-chloro-benzenecarboperoxoic acid; palladium on activated charcoal; In dichloromethane; ethyl acetate;

Reference yield:

: 113730-68-0
1-benzyloxycarbonyl-4,5-dimethyl-2-phenyl-1,2-dihydropyridine

: 113730-81-7
2,7-Dimethyl-5-phenyl-[1,4]diazepine-1-carboxylic acid ethyl ester

Guidance literature:: Multi-step reaction with 5 steps

1: CH₂Cl₂ / 22 h / Irradiation

2: 30 percent / benzyltriethylammonium bromide, NaHCO₃ (0.5N) / CH₂Cl₂; H₂O / 5 h / Ambient temperature

3: 83 percent / H₂ / Pd-C (5percent) / ethyl acetate / Ambient temperature

4: 81 percent / tert-butyl hypochlorite, DBU / diethyl ether; dimethylformamide / Ambient temperature

5: 72 percent / acetonitrile / Irradiation

With tert-butylhypochlorite; hydrogen; benzyltriethylammonium bromide; sodium hydrogencarbonate; 1,8-diazabicyclo[5.4.0]undec-7-ene; palladium on activated charcoal; In diethyl ether; dichloromethane; water; ethyl acetate; N,N-dimethyl-formamide; acetonitrile;