3-Buten-2-one,4-[(1S,2R,4S)-4-(acetyloxy)-2-hydroxy-2,6,6-trimethylcyclohexylidene]-, (3S)-

Base Information

Chemical Name:3-Buten-2-one,4-[(1S,2R,4S)-4-(acetyloxy)-2-hydroxy-2,6,6-trimethylcyclohexylidene]-, (3S)-
CAS No.:26289-05-4
Molecular Formula:C₁₅H₂₂O₄
Molecular Weight:266.337
Hs Code.:

Synonyms:3-Buten-2-one,4-(2,4-dihydroxy-2,6,6-trimethylcyclohexylidene)-, 4-acetate, stereoisomer(8CI); 3-Buten-2-one,4-[4-(acetyloxy)-2-hydroxy-2,6,6-trimethylcyclohexylidene]-, [2R-(1R*,2a,4b)]-; Apo-9'-fucoxanthinone

Suppliers and Price of 3-Buten-2-one,4-[(1S,2R,4S)-4-(acetyloxy)-2-hydroxy-2,6,6-trimethylcyclohexylidene]-, (3S)-

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
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price

Total 8 raw suppliers

Chemical Property of 3-Buten-2-one,4-[(1S,2R,4S)-4-(acetyloxy)-2-hydroxy-2,6,6-trimethylcyclohexylidene]-, (3S)-

Chemical Property:

Purity/Quality:: 99% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 3-Buten-2-one,4-[(1S,2R,4S)-4-(acetyloxy)-2-hydroxy-2,6,6-trimethylcyclohexylidene]-, (3S)-

There total 10 articles about 3-Buten-2-one,4-[(1S,2R,4S)-4-(acetyloxy)-2-hydroxy-2,6,6-trimethylcyclohexylidene]-, (3S)- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 24.0%

: <3R-<1β,3α,4R*(3E,5E,7E,9E)>>-3-Hydroxy-4-(3,10-dimethyl-11-phenylsulfonylundeca-1,3,5,7,9-pentaenylidene)-3,5,5-trimethylcyclohexyl acetate

: 22451-58-7,22488-60-4,26289-05-4,130321-04-9,130321-06-1,130321-07-2
3'R,4'-<(2R,4S)-2-hydroxy-4-acetoxy-2,6,6-trimethylcyclohexylidene>but-3'-en-2'-one

Guidance literature:: With ozone; In methanol; at -78 ℃;

Reference yield: 6.9%

: 3351-86-8,17257-05-5,55659-36-4,55659-37-5,55659-38-6,92761-37-0,124378-42-3,138126-73-5,141270-13-5,141270-14-6,141270-15-7,141270-16-8
fucoxanthin

: 22451-58-7,22488-60-4,26289-05-4,130321-04-9,130321-06-1,130321-07-2
3'R,4'-<(2R,4S)-2-hydroxy-4-acetoxy-2,6,6-trimethylcyclohexylidene>but-3'-en-2'-one

: apo-13-fucoxanthinone

Guidance literature:: With ozone; In methanol; dichloromethane; at 0 ℃; for 2h;
DOI:10.3390/md16080275

Reference yield:

: peridinin p-bromobenzoate

: 22451-58-7,22488-60-4,26289-05-4,130321-04-9,130321-06-1,130321-07-2
3'R,4'-<(2R,4S)-2-hydroxy-4-acetoxy-2,6,6-trimethylcyclohexylidene>but-3'-en-2'-one

: 8-p-bromobenzoyloxy-5,6-epoxy-β-cyclocitral

Guidance literature:: With ozone; In ethyl acetate; at -78 ℃; for 0.15h; Yield given. Yields of byproduct given;
DOI:10.1016/0031-9422(80)83197-9