pyridoxal 4-methoxybenzoyl hydrazone

Base Information

• Chemical Name: pyridoxal 4-methoxybenzoyl hydrazone
• CAS No.: 116324-89-1
• Molecular Formula: C16H17 N3 O4
• Molecular Weight: 315.32
• Mol file: 116324-89-1.mol

Synonyms:Benzoicacid, 4-methoxy-, [[3-hydroxy-5-(hydroxymethyl)-2-methyl-4-pyridinyl]methylene]hydrazide(9CI); Pyridoxal (4-methoxybenzoyl)hydrazone

Chemical Property of pyridoxal 4-methoxybenzoyl hydrazone

Chemical Property:

• Boiling Point: °Cat760mmHg
• Flash Point: °C
• PSA: 104.04000
• Density: 1.29g/cm³
• LogP: 1.75130

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of pyridoxal 4-methoxybenzoyl hydrazone

There total 3 articles about pyridoxal 4-methoxybenzoyl hydrazone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

pyridoxal hydrochloride (65-22-5) + 4-methoxybenzoic acid hydrazide (3290-99-1) → 4-Methoxy-benzoic acid [1-(3-hydroxy-5-hydroxymethyl-2-methyl-pyridin-4-yl)-meth-(E)-ylidene]-hydrazide (116324-89-1)

Guidance literature:

With sodium acetate; In water; for 0.5h; Heating;

DOI:10.1021/je00054a044

Reference yield:

pyridoxal (66-72-8) + 4-methoxybenzoic acid hydrazide (3290-99-1) → C16H17N3O4 (116324-89-1)

Guidance literature:

In methanol; at 20 ℃;

DOI:10.1016/j.jorganchem.2012.02.010

Reference yield:

pyridoxal (66-72-8) + 4-methoxybenzoic acid hydrazide (3290-99-1) → 4-Methoxy-benzoic acid [1-(3-hydroxy-5-hydroxymethyl-2-methyl-pyridin-4-yl)-meth-(E)-ylidene]-hydrazide (116324-89-1)

Guidance literature:

upstream raw materials:

pyridoxal

4-methoxybenzoic acid hydrazide

pyridoxal hydrochloride

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