Jolkinolide B

Base Information

Chemical Name:Jolkinolide B
CAS No.:37905-08-1
Molecular Formula:C20H26O4
Molecular Weight:330.41800
Hs Code.:
NSC Number:700087
DSSTox Substance ID:DTXSID70958923
Nikkaji Number:J18.288E
Wikidata:Q27138168
Metabolomics Workbench ID:133762
ChEMBL ID:CHEMBL404387
Mol file:37905-08-1.mol

Synonyms:jolkinolide B

Suppliers and Price of Jolkinolide B

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Usbiological
Jolkinolide B
10mg
$ 468.00

Biorbyt Ltd
Jolkinolide B 98%
20 mg
$ 634.10

Biorbyt Ltd
Jolkinolide B 98%
10 mg
$ 499.80

AvaChem
Jolkinolide B
100mg
$ 1190.00

AvaChem
Jolkinolide B
5mg
$ 190.00

AvaChem
Jolkinolide B
20mg
$ 390.00

Arctom
JolkinolideB ≥98%
20mg
$ 343.00

ApexBio Technology
JolkinolideB
20mg
$ 250.00

Total 29 raw suppliers

Chemical Property of Jolkinolide B

Chemical Property:

Vapor Pressure:5.08E-10mmHg at 25°C
Melting Point:213-215℃
Boiling Point:497.1oC at 760 mmHg
Flash Point:219.8oC
PSA：51.36000
Density:1.28g/cm3
LogP:3.34860
XLogP3:3.2
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:4
Rotatable Bond Count:0
Exact Mass:330.18310931
Heavy Atom Count:24
Complexity:723

Purity/Quality:

HPLC≥98% ^*data from raw suppliers

Jolkinolide B ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CC1=C2C3C4(O3)CCC5C(CCCC5(C4C6C2(O6)OC1=O)C)(C)C
Isomeric SMILES:CC1=C2[C@@H]3[C@]4(O3)CC[C@H]5[C@]([C@@H]4[C@@H]6[C@]2(O6)OC1=O)(CCCC5(C)C)C

Technology Process of Jolkinolide B

There total 6 articles about Jolkinolide B which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 84.0%

: 37905-07-0,86746-85-2,97906-88-2
jolkinolide A

: 86746-86-3,97906-89-3,37905-08-1
jolkinolide B

Guidance literature:: With dihydrogen peroxide; sodium hydroxide; In methanol; at 20 ℃; Cooling with ice;

Reference yield: 76.2%

: 37905-07-0,86746-85-2,97906-88-2
jolkinolide A

: 37905-08-1,86746-86-3,97906-89-3
jolkinolide B

Guidance literature:: With 3-chloro-benzenecarboperoxoic acid; In dichloromethane; Ambient temperature;
DOI:10.1016/0040-4020(89)80132-2

Reference yield:

: ent-8β,14β-epoxy-12-hydroxypodocarp-11(12)-en-13-one

: 86746-86-3,97906-89-3,37905-08-1
jolkinolide B

Guidance literature:: Multi-step reaction with 3 steps

2: NaH / 1,2-dimethoxy-ethane / 0.08 h / Ambient temperature

3: m-chloroperbenzoic acid

With sodium hydride; 3-chloro-benzenecarboperoxoic acid; In 1,2-dimethoxyethane;
DOI:10.1039/c39830000330