3-Cyclopenten-1-one, 2-[[5-(4-morpholinyl)-1-(4-nitrophenyl)-1H-1,2,3-triazol-4-yl]methyl]-2,3,4 ,5-tetraphenyl-, trans-

Base Information

• Chemical Name: 3-Cyclopenten-1-one, 2-[[5-(4-morpholinyl)-1-(4-nitrophenyl)-1H-1,2,3-triazol-4-yl]methyl]-2,3,4 ,5-tetraphenyl-, trans-
• CAS No.: 114026-64-1
• Molecular Formula: C₄₂H₃₅N₅O₄
• Molecular Weight: 673.771
• Mol file: 114026-64-1.mol

Synonyms:

Chemical Property of 3-Cyclopenten-1-one, 2-[[5-(4-morpholinyl)-1-(4-nitrophenyl)-1H-1,2,3-triazol-4-yl]methyl]-2,3,4 ,5-tetraphenyl-, trans-

Chemical Property:

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Technology Process of 3-Cyclopenten-1-one, 2-[[5-(4-morpholinyl)-1-(4-nitrophenyl)-1H-1,2,3-triazol-4-yl]methyl]-2,3,4 ,5-tetraphenyl-, trans-

There total 10 articles about 3-Cyclopenten-1-one, 2-[[5-(4-morpholinyl)-1-(4-nitrophenyl)-1H-1,2,3-triazol-4-yl]methyl]-2,3,4 ,5-tetraphenyl-, trans- which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

C42H35N5O4 (105808-38-6,107133-75-5,114128-86-8) → (2S,5R)-2-[5-Morpholin-4-yl-1-(4-nitro-phenyl)-1H-[1,2,3]triazol-4-ylmethyl]-2,3,4,5-tetraphenyl-cyclopent-3-enone (105808-39-7,114026-64-1)

Guidance literature:

In chloroform; for 216h; Ambient temperature;

DOI:10.1016/S0040-4020(01)87401-9

Reference yield: 45.0%

4-nitrophenyl azide (1516-60-5) + 5-morpholinomethylene-1,2,3,4-tetraphenyl-bicyclo(2.2.1)hept-2-en-7-one (107090-34-6,107090-35-7) → (2S,5R)-2-[5-Morpholin-4-yl-1-(4-nitro-phenyl)-1H-[1,2,3]triazol-4-ylmethyl]-2,3,4,5-tetraphenyl-cyclopent-3-enone (105808-39-7,114026-64-1) + C42H35N5O4 (105808-38-6,107133-75-5,114128-86-8)

Guidance literature:

In benzene; for 48h;

DOI:10.1016/S0040-4020(01)87401-9

Reference yield: 30.0%

4,5-Dihydro-4-methylene-5-morpholino-1-(4-nitrophenyl)-ν-triazole (74073-15-7) + 2,3,4,5-tetraphenylcyclopenta-2,4-dienone (479-33-4) → (2S,5R)-2-[5-Morpholin-4-yl-1-(4-nitro-phenyl)-1H-[1,2,3]triazol-4-ylmethyl]-2,3,4,5-tetraphenyl-cyclopent-3-enone (105808-39-7,114026-64-1) + C42H35N5O4 (105808-38-6,107133-75-5,114128-86-8)

Guidance literature:

In dichloromethane; at 5 ℃; for 72h;

DOI:10.1016/S0040-4020(01)87400-7

upstream raw materials:

(2S,5R)-2-[5-Morpholin-4-yl-1-(4-nitro-phenyl)-1H-[1,2,3]triazol-4-ylmethyl]-2,3,4,5-tetraphenyl-cyclopent-3-enone

C₄₂H₃₅N₅O₄

morpholine

4-nitrophenyl azide

Downstream raw materials:

(4R^*,5R^*)-5-<5-morpholino-1-(4-nitrophenyl)-v-triazol-4-yl>methyl-2,3,4,5-tetraphenyl-2-cyclopent-1-one

5-hydroperoxy-2-<5-morpholino-1-(4-nitrophenyl)-v-triazol-4-yl>methyl-2,3,4,5-tetraphenyl-3-cyclopenten-1-one

(2S^*,5S^*)-2-<5-morpholino-1-(4-nitrophenyl)-v-triazol-4-yl>methyl-2,3,4,5-tetraphenyl-3-cyclopenten-1-one

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