Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[trimethylsilyl bis(1-methylethyl)phosphoramidite]

Base Information

Chemical Name:Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[trimethylsilyl bis(1-methylethyl)phosphoramidite]
CAS No.:114071-81-7
Molecular Formula:C₃₂H₅₃N₆O₅PSi₂
Molecular Weight:688.955
Hs Code.:
Mol file:114071-81-7.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[trimethylsilyl bis(1-methylethyl)phosphoramidite]

Chemical Property:

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Technology Process of Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[trimethylsilyl bis(1-methylethyl)phosphoramidite]

There total 1 articles about Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[trimethylsilyl bis(1-methylethyl)phosphoramidite] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114071-78-2
trimethylsilyl N,N,N',N'-tetraisopropylphosphorodiamidite

: 51549-39-4
N⁶-benzoyl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

: 114071-81-7
C₃₂H₅₃N₆O₅PSi₂

Guidance literature:: DOI:10.1016/S0040-4039(00)95534-5

Reference yield:

: 114071-81-7
C₃₂H₅₃N₆O₅PSi₂

: 114071-85-1
C₂₉H₄₄ClN₆O₅PSi

Guidance literature:: With sulfuryl dichloride; In dichloromethane; 1.) 0 deg C, 2.) 30 min, room temperature;
DOI:10.1016/S0040-4039(00)95534-5

Reference yield:

: 114071-81-7
C₃₂H₅₃N₆O₅PSi₂

: 114071-89-5
Benzoic acid (2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-{[(2R,3S,5R)-5-(6-benzoylamino-purin-9-yl)-2-(tert-butyl-dimethyl-silanyloxymethyl)-tetrahydro-furan-3-yloxy]-diisopropylamino-phosphoryloxymethyl}-tetrahydro-furan-3-yl ester

Guidance literature:: Multi-step reaction with 2 steps

1: sulfuryl chloride / CH₂Cl₂ / 1.) 0 deg C, 2.) 30 min, room temperature

2: triethylamine / CH₂Cl₂ / 1 h

With sulfuryl dichloride; triethylamine; In dichloromethane;
DOI:10.1016/S0040-4039(00)95534-5