Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[bis(1-methylethyl)phosphoramidochloridate]

Base Information

Chemical Name:Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[bis(1-methylethyl)phosphoramidochloridate]
CAS No.:114071-85-1
Molecular Formula:C₂₉H₄₄ClN₆O₅PSi
Molecular Weight:651.218
Hs Code.:
Mol file:114071-85-1.mol

Synonyms:

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[bis(1-methylethyl)phosphoramidochloridate]

Chemical Property:

Purity/Quality:

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Technology Process of Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[bis(1-methylethyl)phosphoramidochloridate]

There total 3 articles about Adenosine, N-benzoyl-2'-deoxy-5'-O-[(1,1-dimethylethyl)dimethylsilyl]-, 3'-[bis(1-methylethyl)phosphoramidochloridate] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 114071-81-7
C₃₂H₅₃N₆O₅PSi₂

: 114071-85-1
C₂₉H₄₄ClN₆O₅PSi

Guidance literature:: With sulfuryl dichloride; In dichloromethane; 1.) 0 deg C, 2.) 30 min, room temperature;
DOI:10.1016/S0040-4039(00)95534-5

Reference yield:

: 114071-78-2
trimethylsilyl N,N,N',N'-tetraisopropylphosphorodiamidite

: 114071-85-1
C₂₉H₄₄ClN₆O₅PSi

Guidance literature:: Multi-step reaction with 2 steps

2: sulfuryl chloride / CH₂Cl₂ / 1.) 0 deg C, 2.) 30 min, room temperature

With sulfuryl dichloride; In dichloromethane;
DOI:10.1016/S0040-4039(00)95534-5

Reference yield:

: 51549-39-4
N⁶-benzoyl-5′-O-(tert-butyldimethylsilyl)-2′-deoxyadenosine

: 114071-85-1
C₂₉H₄₄ClN₆O₅PSi

Guidance literature:: Multi-step reaction with 2 steps

2: sulfuryl chloride / CH₂Cl₂ / 1.) 0 deg C, 2.) 30 min, room temperature

With sulfuryl dichloride; In dichloromethane;
DOI:10.1016/S0040-4039(00)95534-5