Technology Process of 2-(2-Phenylethyl)chromone
There total 9 articles about 2-(2-Phenylethyl)chromone which
guide to synthetic route it.
The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:
synthetic route:
- Guidance literature:
-
o-hydroxyacetophenone; 3-phenylpropanoate;
With
sodium hydride;
In
tetrahydrofuran; mineral oil;
for 0.0833333h;
Reflux;
Inert atmosphere;
With
hydrogenchloride;
In
methanol; water;
at 20 ℃;
for 14h;
Inert atmosphere;
DOI:10.1039/c8cc07787h
- Guidance literature:
-
With
chlorocarbonylbis(triphenylphosphine)rhodium(I); potassium carbonate;
In
N,N-dimethyl acetamide;
at 90 ℃;
for 5h;
Schlenk technique;
Inert atmosphere;
DOI:10.1039/c9ob02670c
- Guidance literature:
-
With
hydrogenchloride; acetic acid;
In
water;
Reflux;
